3,4'-bis(4-nitrobenzoyloxy)-3'-fluorobiphenyl

Base Information

Chemical Name:3,4'-bis(4-nitrobenzoyloxy)-3'-fluorobiphenyl
CAS No.:1287777-13-2
Molecular Formula:C₂₆H₁₅FN₂O₈
Molecular Weight:502.412
Hs Code.:

Synonyms:3,4'-bis(4-nitrobenzoyloxy)-3'-fluorobiphenyl

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Chemical Property of 3,4'-bis(4-nitrobenzoyloxy)-3'-fluorobiphenyl

Chemical Property:

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Technology Process of 3,4'-bis(4-nitrobenzoyloxy)-3'-fluorobiphenyl

There total 7 articles about 3,4'-bis(4-nitrobenzoyloxy)-3'-fluorobiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 406482-59-5
3'-fluoro-biphenyl-3,4'-diol

: 62-23-7
4-nitro-benzoic acid

: 1287777-13-2
3,4'-bis(4-nitrobenzoyloxy)-3'-fluorobiphenyl

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1002/jccs.201000020

Reference yield:

: 188595-15-5
2-(4-bromo-2-fluorophenoxy)tetrahydro-2H-pyran

: 1287777-13-2
3,4'-bis(4-nitrobenzoyloxy)-3'-fluorobiphenyl

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / ethanol; toluene / 5 h / 90 °C

2: toluene-4-sulfonic acid / methanol; dichloromethane; water / 50 °C

3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 12 h / 20 °C

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In methanol; ethanol; dichloromethane; water; toluene; 1: Suzuki coupling;
DOI:10.1002/jccs.201000020

Reference yield:

: 1287777-05-2
[3-(tetrahydro-2H-pyran-2-yloxy)phenyl]boronic acid

: 1287777-13-2
3,4'-bis(4-nitrobenzoyloxy)-3'-fluorobiphenyl

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / ethanol; toluene / 5 h / 90 °C

2: toluene-4-sulfonic acid / methanol; dichloromethane; water / 50 °C

3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 12 h / 20 °C

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In methanol; ethanol; dichloromethane; water; toluene; 1: Suzuki coupling;
DOI:10.1002/jccs.201000020