2-(N-benzyloxycarbonyl)-aminoethyl (4-N-azido-4-deoxy-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

Base Information

Chemical Name:2-(N-benzyloxycarbonyl)-aminoethyl (4-N-azido-4-deoxy-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside
CAS No.:1388133-70-7
Molecular Formula:C₉₁H₇₈N₄O₂₆
Molecular Weight:1643.63
Hs Code.:

2-(N-benzyloxycarbonyl)-aminoethyl (4-N-azido-4-deoxy-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

Synonyms:2-(N-benzyloxycarbonyl)-aminoethyl (4-N-azido-4-deoxy-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

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Chemical Property of 2-(N-benzyloxycarbonyl)-aminoethyl (4-N-azido-4-deoxy-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

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Technology Process of 2-(N-benzyloxycarbonyl)-aminoethyl (4-N-azido-4-deoxy-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

There total 1 articles about 2-(N-benzyloxycarbonyl)-aminoethyl (4-N-azido-4-deoxy-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1388133-63-8
ethyl 4-deoxy-4-azido-2,3,6-tri-O-benzoyl-β-D-thio-glucopyranoside

: C₅₇H₅₃NO₁₈

: 98-88-4
benzoyl chloride

: 1388133-70-7
2-(N-benzyloxycarbonyl)-aminoethyl (4-N-azido-4-deoxy-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

Guidance literature:: ethyl 4-deoxy-4-azido-2,3,6-tri-O-benzoyl-β-D-thio-glucopyranoside; C₅₇H₅₃NO₁₈; With N-iodo-succinimide; silver trifluoromethanesulfonate; In dichloromethane; at 0 - 20 ℃; for 1h; Molecular sieve;

benzoyl chloride; With pyridine; In dichloromethane; for 2h;
DOI:10.1016/j.tet.2012.05.118

Reference yield: 65.0%

: 4530-20-5
BOC-glycine

: 1388133-70-7
2-(N-benzyloxycarbonyl)-aminoethyl (4-N-azido-4-deoxy-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside

: 1381880-16-5
2-(N-benzyloxycarbonyl)-aminoethyl (4-deoxy-4-N-tert-butyloxycarbonyl-glycyl-β-D-glucopyranosyl)-(1->3)-(β-D-galactopyranosyl)-(1->4)-β-D-glucopyranoside

Guidance literature:: 2-(N-benzyloxycarbonyl)-aminoethyl (4-N-azido-4-deoxy-2,3,6-tri-O-benzoyl-β-D-glucopyranosyl)-(1->3)-(2,4,6-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzoyl-β-D-glucopyranoside; With sodium methylate; In methanol; dichloromethane; for 3h;

In methanol; dichloromethane;

BOC-glycine; Further stages;
DOI:10.1016/j.tet.2012.05.118