methyl [p-methylphenyl 7-O-acetyl-4,8,9-tri-O-benzoyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside]onate

Base Information

• Chemical Name: methyl [p-methylphenyl 7-O-acetyl-4,8,9-tri-O-benzoyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside]onate
• CAS No.: 1356459-42-1
• Molecular Formula: C₄₂H₄₁NO₁₂S
• Molecular Weight: 783.853

Synonyms:methyl [p-methylphenyl 7-O-acetyl-4,8,9-tri-O-benzoyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside]onate

Chemical Property of methyl [p-methylphenyl 7-O-acetyl-4,8,9-tri-O-benzoyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside]onate

Chemical Property:

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Technology Process of methyl [p-methylphenyl 7-O-acetyl-4,8,9-tri-O-benzoyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside]onate

There total 3 articles about methyl [p-methylphenyl 7-O-acetyl-4,8,9-tri-O-benzoyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside]onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

methyl [p-methylphenyl 5-acetamido-4,8,9-tri-O-benzoyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside]onate (1356459-41-0) + acetic anhydride (108-24-7) → methyl [p-methylphenyl 7-O-acetyl-4,8,9-tri-O-benzoyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside]onate (1356459-42-1)

Guidance literature:

In pyridine; Inert atmosphere;

DOI:10.1021/ol3000475

Reference yield:

benzoyl chloride (98-88-4) → methyl [p-methylphenyl 7-O-acetyl-4,8,9-tri-O-benzoyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside]onate (1356459-42-1)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 5 h / 0 °C

2: pyridine / Inert atmosphere

With pyridine; In pyridine;

DOI:10.1021/ol3000475

Reference yield:

(2R,4S,5R,6R)-5-Acetylamino-4-hydroxy-2-p-tolylsulfanyl-6-((1R,2R)-1,2,3-trihydroxy-propyl)-tetrahydro-pyran-2-carboxylic acid methyl ester → methyl [p-methylphenyl 7-O-acetyl-4,8,9-tri-O-benzoyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside]onate (1356459-42-1)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 5 h / 0 °C

2: pyridine / Inert atmosphere

With pyridine; In pyridine;

DOI:10.1021/ol3000475

upstream raw materials:

methyl [p-methylphenyl 5-acetamido-4,8,9-tri-O-benzoyl-3,5-dideoxy-2-thio-D-glycero-β-D-galacto-non-2-ulopyranoside]onate

acetic anhydride

benzoyl chloride

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