tert-butyl N-[3-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]propyl]carbamate

Base Information

Chemical Name:tert-butyl N-[3-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]propyl]carbamate
CAS No.:1201790-19-3
Molecular Formula:C₂₀H₃₂BNO₅
Molecular Weight:377.289
Hs Code.:

Synonyms:tert-butyl N-[3-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]propyl]carbamate

Suppliers and Price of tert-butyl N-[3-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]propyl]carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of tert-butyl N-[3-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]propyl]carbamate

Chemical Property:

Purity/Quality:: 99%,98%, ^*data from raw suppliers

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Technology Process of tert-butyl N-[3-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]propyl]carbamate

There total 8 articles about tert-butyl N-[3-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]propyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.4%

: 83948-53-2
3-bromopropylamine tert-butylcarbamate

: 269409-70-3
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol

: 1201790-19-3
tert-butyl N-[3-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]propyl]carbamate

Guidance literature:: With potassium carbonate; In acetonitrile; at 65 ℃; for 12h;

Reference yield: 67.5%

: 116861-31-5
tert-butyl N-(3-chloropropyl)carbamate

: 269409-70-3
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol

: 1201790-19-3
tert-butyl N-[3-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]propyl]carbamate

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In butanone; for 24h; Reflux; Inert atmosphere;
DOI:10.1002/adma.201202673

Reference yield:

: 34619-03-9
tert-butyldicarbonate

: 1201790-19-3
tert-butyl N-[3-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]propyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0 °C

2: potassium carbonate; 18-crown-6 ether / butanone / 24 h / Reflux; Inert atmosphere

With 18-crown-6 ether; potassium carbonate; triethylamine; In dichloromethane; butanone;
DOI:10.1002/adma.201202673