2-amino-6-sulfanyl-4-[4-(2,2,2-trifluoroethoxy)phenyl]pyridine-3,5-dicarbonitrile

Base Information

Chemical Name:2-amino-6-sulfanyl-4-[4-(2,2,2-trifluoroethoxy)phenyl]pyridine-3,5-dicarbonitrile
CAS No.:1353657-23-4
Molecular Formula:C₁₅H₉F₃N₄OS
Molecular Weight:350.324
Hs Code.:

Synonyms:2-amino-6-sulfanyl-4-[4-(2,2,2-trifluoroethoxy)phenyl]pyridine-3,5-dicarbonitrile

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Chemical Property of 2-amino-6-sulfanyl-4-[4-(2,2,2-trifluoroethoxy)phenyl]pyridine-3,5-dicarbonitrile

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Technology Process of 2-amino-6-sulfanyl-4-[4-(2,2,2-trifluoroethoxy)phenyl]pyridine-3,5-dicarbonitrile

There total 1 articles about 2-amino-6-sulfanyl-4-[4-(2,2,2-trifluoroethoxy)phenyl]pyridine-3,5-dicarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 7357-70-2
Cyanothioacetamide

: 76579-46-9
4-(2,2,2-trifluoroethoxy)benzaldehyde

: 1353657-23-4
2-amino-6-sulfanyl-4-[4-(2,2,2-trifluoroethoxy)phenyl]pyridine-3,5-dicarbonitrile

Guidance literature:: With 4-methyl-morpholine; In ethanol; at 20 ℃; for 24h;

Reference yield: 61.0%

: 1353657-23-4
2-amino-6-sulfanyl-4-[4-(2,2,2-trifluoroethoxy)phenyl]pyridine-3,5-dicarbonitrile

: 1353657-34-7
rac-4-(1-chloroethyl)-N-methylpyridine-2-carboxamide trifluoroacetate

: 1353656-75-3
rac-4-[1-({6-amino-3,5-dicyano-4-[4-(2,2,2-trifluoroethoxy)phenyl]pyridin-2-yl}sulfanyl)ethyl]-N-methylpyridine-2-carboxamide

Guidance literature:: With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 1353657-23-4
2-amino-6-sulfanyl-4-[4-(2,2,2-trifluoroethoxy)phenyl]pyridine-3,5-dicarbonitrile

: 1353657-34-7
rac-4-(1-chloroethyl)-N-methylpyridine-2-carboxamide trifluoroacetate

: 4-[1-({6-amino-3,5-dicyano-4-[4-(2,2,2-trifluoroethoxy)phenyl]pyridin-2-yl}sulfanyl)ethyl]-N-methylpyridine-2-carboxamide

: 4-[1-({6-amino-3,5-dicyano-4-[4-(2,2,2-trifluoroethoxy)phenyl]pyridin-2-yl}sulfanyl)ethyl]-N-methylpyridine-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 20 °C

2: Chiralcel OD-H / ethanol; 2-Methylpentane / 40 °C / Resolution of racemate

With sodium hydrogencarbonate; In ethanol; 2-Methylpentane; N,N-dimethyl-formamide;