methyl (S)-1-ethyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylate

Base Information

Chemical Name:methyl (S)-1-ethyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylate
CAS No.:1004308-78-4
Molecular Formula:C₁₅H₁₈N₂O₃
Molecular Weight:274.32
Hs Code.:

Synonyms:methyl (S)-1-ethyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (S)-1-ethyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylate

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Technology Process of methyl (S)-1-ethyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylate

There total 1 articles about methyl (S)-1-ethyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 921767-12-6
(benzenesulfonyl-phenyl-methyl)-carbamic acid allyl ester

: 105-45-3
acetoacetic acid methyl ester

: 109-90-0
ethyl isocyanate

: 1004308-78-4
methyl (S)-1-ethyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylate

: methyl (R)-1-ethyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylate

Guidance literature:: (benzenesulfonyl-phenyl-methyl)-carbamic acid allyl ester; acetoacetic acid methyl ester; With sodium carbonate; sodium chloride; Cinchonin; In dichloromethane; water; at -15 ℃; for 48h;

ethyl isocyanate; With 1,3-dimethylbarbituric acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃;

With acetic acid; In ethanol; at 100 ℃; for 0.0833333h; Further stages. Title compound not separated from byproducts.; microwave irradiation;
DOI:10.1021/jo701777g