(benzenesulfonyl-phenyl-methyl)-carbamic acid allyl ester

Base Information

Chemical Name:(benzenesulfonyl-phenyl-methyl)-carbamic acid allyl ester
CAS No.:921767-12-6
Molecular Formula:C₁₇H₁₇NO₄S
Molecular Weight:331.392
Hs Code.:

Synonyms:(benzenesulfonyl-phenyl-methyl)-carbamic acid allyl ester

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Chemical Property of (benzenesulfonyl-phenyl-methyl)-carbamic acid allyl ester

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Technology Process of (benzenesulfonyl-phenyl-methyl)-carbamic acid allyl ester

There total 1 articles about (benzenesulfonyl-phenyl-methyl)-carbamic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 2114-11-6
allyl carbamate

: 873-55-2
sodium benzenesulfonate

: 100-52-7
benzaldehyde

: 921767-12-6
(benzenesulfonyl-phenyl-methyl)-carbamic acid allyl ester

Guidance literature:: allyl carbamate; sodium benzenesulfonate; In methanol; water; at 20 ℃; for 0.0833333h;

benzaldehyde; With formic acid; In methanol; water; at 21 - 22 ℃; for 96h;
DOI:10.15227/orgsyn.086.0236

Reference yield: 96.0%

: 921767-12-6
(benzenesulfonyl-phenyl-methyl)-carbamic acid allyl ester

: 762-72-1
allyl-trimethyl-silane

: 742081-27-2
allyl 1-phenylbut-3-enylcarbamate

Guidance literature:: With Bi(OTF)3*4H₂O; In dichloromethane; at 40 ℃; for 23h; chemoselective reaction; Inert atmosphere;
DOI:10.1002/adsc.200900710

Reference yield:

: 921767-12-6
(benzenesulfonyl-phenyl-methyl)-carbamic acid allyl ester

: 105-45-3
acetoacetic acid methyl ester

: 109-90-0
ethyl isocyanate

: 1004308-78-4
methyl (S)-1-ethyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylate

: methyl (R)-1-ethyl-6-methyl-2-oxo-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylate

Guidance literature:: (benzenesulfonyl-phenyl-methyl)-carbamic acid allyl ester; acetoacetic acid methyl ester; With sodium carbonate; sodium chloride; Cinchonin; In dichloromethane; water; at -15 ℃; for 48h;

ethyl isocyanate; With 1,3-dimethylbarbituric acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃;

With acetic acid; In ethanol; at 100 ℃; for 0.0833333h; Further stages. Title compound not separated from byproducts.; microwave irradiation;
DOI:10.1021/jo701777g