N-METHYL DIISOBUTYLAMINE

Base Information

• Chemical Name: N-METHYL DIISOBUTYLAMINE
• CAS No.: 10471-20-2
• Molecular Formula: C₉H₂₁N
• Molecular Weight: 143.272
• Hs Code.: 2921199090
• Mol file: 10471-20-2.mol

Synonyms:Dipropylamine,N,2,2'-trimethyl- (6CI,7CI,8CI); Diisobutylmethylamine;N,2,2'-Trimethyldipropylamine; N,N-Bis(2-methylpropyl)methylamine

Chemical Property of N-METHYL DIISOBUTYLAMINE

Chemical Property:

• PSA: 3.24000
• LogP: 2.23020

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-METHYL DIISOBUTYLAMINE

There total 3 articles about N-METHYL DIISOBUTYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

→ diisobutyl-methyl-amine (10471-20-2)

Guidance literature:

With (CuAl)O(x); hydrogen; In tetrahydrofuran; at 140 ℃; for 9h; under 3750.38 Torr;

Reference yield: 66.0%

isopropylmagnesium bromide (920-39-8) + N,N-bis[(benzotriazol-1-yl)methyl]methylamine (111184-77-1) → diisobutyl-methyl-amine (10471-20-2)

Guidance literature:

In tetrahydrofuran; for 1h; Heating;

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + diisobutylamine (110-96-3) → diisobutyl-methyl-amine (10471-20-2)

Guidance literature:

With formic acid;

DOI:10.1021/jo50006a014

upstream raw materials:

formaldehyd

diisobutylamine

isopropylmagnesium bromide

N,N-bis[(benzotriazol-1-yl)methyl]methylamine

Refernces

• 1、 -. "Method for selectively preparing N-monomethylamine compound". Paragraph 0034-0035. . Retrieved 2017/08/29.