4-(2,2,3,3,4,4,5,5-Octafluoropentoxy)-2,3,5,6-tetrafluorophenylacetylene

Base Information

Chemical Name:4-(2,2,3,3,4,4,5,5-Octafluoropentoxy)-2,3,5,6-tetrafluorophenylacetylene
CAS No.:365564-82-5
Molecular Formula:C₁₃H₄F₁₂O
Molecular Weight:404.155
Hs Code.:

Synonyms:4-(2,2,3,3,4,4,5,5-Octafluoropentoxy)-2,3,5,6-tetrafluorophenylacetylene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(2,2,3,3,4,4,5,5-Octafluoropentoxy)-2,3,5,6-tetrafluorophenylacetylene

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Technology Process of 4-(2,2,3,3,4,4,5,5-Octafluoropentoxy)-2,3,5,6-tetrafluorophenylacetylene

There total 1 articles about 4-(2,2,3,3,4,4,5,5-Octafluoropentoxy)-2,3,5,6-tetrafluorophenylacetylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 355-80-6
2,2,3,3,4,4,5,5-octafluoropentan-1-ol

: 52168-00-0
((trimethylsilyl)ethynyl)pentafluorobenzene

: 365564-82-5
4-(2,2,3,3,4,4,5,5-Octafluoropentoxy)-2,3,5,6-tetrafluorophenylacetylene

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1016/S0022-1139(01)00403-1

Reference yield: 90.0%

: 365564-82-5
4-(2,2,3,3,4,4,5,5-Octafluoropentoxy)-2,3,5,6-tetrafluorophenylacetylene

: 4-(6-Chloro-3,3,4,4,5,5,6,6-octafluorohexoxycarbonyl)phenyl 4-iodobenzoate

: 4-(6-Chloro-3,3,4,4,5,5,6,6-octafluorohexoxycarbonyl)phenyl 4-[4-(2,2,3,3,4,4,5,5-octafluoropentoxy-2,3,5,6-tetrafluorophenyl)ethynyl]benzoate

Guidance literature:: With triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; at 60 ℃; for 48h;
DOI:10.1016/S0022-1139(01)00403-1

Reference yield:

: 1-iodo-4-[(S)-2-methylbutoxycarbonyl]benzene

: 365564-82-5
4-(2,2,3,3,4,4,5,5-Octafluoropentoxy)-2,3,5,6-tetrafluorophenylacetylene

: (S)-2-Methylbutyl 4-[4-(2,2,3,3,4,4,5,5-octafluoropentoxy-2,3,5,6-tetrafluorophenyl)ethynyl]benzoate

Guidance literature:: With triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; at 60 ℃; for 48h;
DOI:10.1016/S0022-1139(01)00403-1