Technology Process of C12H13N3O4S2
There total 4 articles about C12H13N3O4S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
water; acetonitrile;
for 2.83333h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium carbonate / dimethyl sulfoxide / 1 h / 35 °C
1.2: 58 °C
2.1: dihydrogen peroxide / sodium tungstate (VI) dihydrate / water; acetic acid / 30 - 60 °C
3.1: trichlorophosphate / acetonitrile; ISOPROPYLAMIDE / 2 h / 45 - 60 °C
4.1: acetonitrile; water / 2.83 h / 5 °C
With
dihydrogen peroxide; lithium carbonate; trichlorophosphate;
sodium tungstate (VI) dihydrate;
In
ISOPROPYLAMIDE; water; acetic acid; dimethyl sulfoxide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dihydrogen peroxide / sodium tungstate (VI) dihydrate / water; acetic acid / 30 - 60 °C
2: trichlorophosphate / acetonitrile; ISOPROPYLAMIDE / 2 h / 45 - 60 °C
3: acetonitrile; water / 2.83 h / 5 °C
With
dihydrogen peroxide; trichlorophosphate;
sodium tungstate (VI) dihydrate;
In
ISOPROPYLAMIDE; water; acetic acid; acetonitrile;