[(η5-C5H5)Fe(1,2-(diphenylphosphino)ethane)(η1-P(basal)-tetraphosphorus trisulfide)] triflate

Base Information

Chemical Name:[(η5-C5H5)Fe(1,2-(diphenylphosphino)ethane)(η1-P(basal)-tetraphosphorus trisulfide)] triflate
CAS No.:1221971-68-1
Molecular Formula:CF₃O₃S*C₃₁H₂₉FeP₆S₃
Molecular Weight:888.529
Hs Code.:

Synonyms:[(η5-C5H5)Fe(1,2-(diphenylphosphino)ethane)(η1-P(basal)-tetraphosphorus trisulfide)] triflate

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Chemical Property of [(η5-C5H5)Fe(1,2-(diphenylphosphino)ethane)(η1-P(basal)-tetraphosphorus trisulfide)] triflate

Chemical Property:

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Technology Process of [(η5-C5H5)Fe(1,2-(diphenylphosphino)ethane)(η1-P(basal)-tetraphosphorus trisulfide)] triflate

There total 1 articles about [(η5-C5H5)Fe(1,2-(diphenylphosphino)ethane)(η1-P(basal)-tetraphosphorus trisulfide)] triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1314-85-8
phosphorus sulfide

: 32843-51-9
[CpFeCl(dppe)]

: 2923-28-6
silver trifluoromethanesulfonate

: 1221971-68-1
[(η5-C5H5)Fe(1,2-(diphenylphosphino)ethane)(η1-P(basal)-tetraphosphorus trisulfide)] triflate

Guidance literature:: In tetrahydrofuran; dichloromethane; (N2); slurry of Fe compd., AgOTf and P4S3 in CH2Cl2/THF stirred for 4 h; mixt. filtered, filtrate evapd. under vac., residue washed with toluene and n-hexane, dried; elem. anal.;
DOI:10.1016/j.jorganchem.2009.12.022

Reference yield:

: 1221971-68-1
[(η5-C5H5)Fe(1,2-(diphenylphosphino)ethane)(η1-P(basal)-tetraphosphorus trisulfide)] triflate

: 7732-18-5
water

: 13598-36-2
phosphonic Acid

: [(η5-C5H5)Fe(1,2-bis(diphenylphosphino)ethane))(HP(OH)2)](1+)

: [(η5-C5H5)Fe(1,2-bis(diphenylphosphino)ethane)(P(OH)3)](1+)

: 6303-21-5
hypophosphorous acid

Guidance literature:: In tetrahydrofuran; Fe compd. in THF hydrolysed with excess of H2O within 1 day; detected by NMR spectroscopy;
DOI:10.1016/j.jorganchem.2009.12.022