2-Benzyl-2,3,6,7,12,12b-hexahydropyrazino<1',2':1,2>pyrido<3,4-b>indol-4(1H)-one

Base Information

• Chemical Name: 2-Benzyl-2,3,6,7,12,12b-hexahydropyrazino<1',2':1,2>pyrido<3,4-b>indol-4(1H)-one
• CAS No.: 137606-58-7
• Molecular Formula: C₂₁H₂₁N₃O
• Molecular Weight: 331.417

Synonyms:2-Benzyl-2,3,6,7,12,12b-hexahydropyrazino<1',2':1,2>pyrido<3,4-b>indol-4(1H)-one

Chemical Property of 2-Benzyl-2,3,6,7,12,12b-hexahydropyrazino<1',2':1,2>pyrido<3,4-b>indol-4(1H)-one

Chemical Property:

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Technology Process of 2-Benzyl-2,3,6,7,12,12b-hexahydropyrazino<1',2':1,2>pyrido<3,4-b>indol-4(1H)-one

There total 3 articles about 2-Benzyl-2,3,6,7,12,12b-hexahydropyrazino<1',2':1,2>pyrido<3,4-b>indol-4(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

tryptamine (61-54-1) + ethyl N-benzyl-N-(2,2-diethoxyethyl)glycinate (134303-01-8) → 1-hydroxymethyl-1,2,3,4-tetrahydro-β-carboline (21236-66-8) + ethyl 2-(benzylamino)acetate (6436-90-4) + 1-(1-Hydroxymethyl-1,2,3,4-tetrahydro-β-carbolin-9-yl)-ethanone + 2-Benzyl-2,3,6,7,12,12b-hexahydropyrazino<1',2':1,2>pyrido<3,4-b>indol-4(1H)-one (137606-58-7)

Guidance literature:

With acetic acid; In water; Yields of byproduct given; Heating;

DOI:10.1016/S0040-4020(01)80944-3

Reference yield:

tryptamine (61-54-1) + ethyl N-benzyl-N-(2,2-diethoxyethyl)glycinate (134303-01-8) + acetic acid (64-19-7,77671-22-8) → 1-hydroxymethyl-1,2,3,4-tetrahydro-β-carboline (21236-66-8) + ethyl 2-(benzylamino)acetate (6436-90-4) + 1-(1-Hydroxymethyl-1,2,3,4-tetrahydro-β-carbolin-9-yl)-ethanone + 2-Benzyl-2,3,6,7,12,12b-hexahydropyrazino<1',2':1,2>pyrido<3,4-b>indol-4(1H)-one (137606-58-7)

Guidance literature:

Yield given. Yields of byproduct given; Heating;

DOI:10.1016/S0040-4020(01)80944-3

Reference yield:

benzyl bromide (100-39-0) + 2,3,6,7,12,12b-Hexahydro-1H-pyrazino[1',2':1,2]pyrido[3,4-b]indol-4-one (106412-98-0) → 2-Benzyl-2,3,6,7,12,12b-hexahydropyrazino<1',2':1,2>pyrido<3,4-b>indol-4(1H)-one (137606-58-7)

Guidance literature:

In methanol; chloroform; for 18h; Yield given; Ambient temperature;

DOI:10.1016/S0040-4020(01)80944-3

upstream raw materials:

tryptamine

ethyl N-benzyl-N-(2,2-diethoxyethyl)glycinate

acetic acid

benzyl bromide

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