2'-chloroethyl 3,4-anhydro-1-O-mesitylenesulphonyl-β-D-tagatopyranoside

Base Information

Chemical Name:2'-chloroethyl 3,4-anhydro-1-O-mesitylenesulphonyl-β-D-tagatopyranoside
CAS No.:99042-66-7
Molecular Formula:C₁₇H₂₃ClO₇S
Molecular Weight:406.884
Hs Code.:

Synonyms:2'-chloroethyl 3,4-anhydro-1-O-mesitylenesulphonyl-β-D-tagatopyranoside

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Chemical Property of 2'-chloroethyl 3,4-anhydro-1-O-mesitylenesulphonyl-β-D-tagatopyranoside

Chemical Property:

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Technology Process of 2'-chloroethyl 3,4-anhydro-1-O-mesitylenesulphonyl-β-D-tagatopyranoside

There total 4 articles about 2'-chloroethyl 3,4-anhydro-1-O-mesitylenesulphonyl-β-D-tagatopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 99042-60-1
2'-chloroethyl 1,4-di-O-mesitylenesulphonyl-β-D-fructopyranoside

: 99042-66-7
2'-chloroethyl 3,4-anhydro-1-O-mesitylenesulphonyl-β-D-tagatopyranoside

Guidance literature:: With sodium methylate; for 0.0833333h; Heating;

Reference yield:

: 57-50-1
Sucrose

: 99042-66-7
2'-chloroethyl 3,4-anhydro-1-O-mesitylenesulphonyl-β-D-tagatopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / hydrogen chloride / ethanol / 15 h

2: 51 percent / pyridine / 96 h / Ambient temperature

3: 75 percent / 0.5M sodium methoxide / 0.08 h / Heating

With pyridine; hydrogenchloride; sodium methylate; In ethanol;

Reference yield:

: 84543-36-2
2'-chloroethyl β-D-fructopyranoside

: 99042-66-7
2'-chloroethyl 3,4-anhydro-1-O-mesitylenesulphonyl-β-D-tagatopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / pyridine / 96 h / Ambient temperature

2: 75 percent / 0.5M sodium methoxide / 0.08 h / Heating

With pyridine; sodium methylate;