(2R,3R,4S)-2-(4-methoxybenzyl)oxymethyl-1,2,4-trihydroxyhexane

Base Information

Chemical Name:(2R,3R,4S)-2-(4-methoxybenzyl)oxymethyl-1,2,4-trihydroxyhexane
CAS No.:113956-98-2
Molecular Formula:C₁₅H₂₄O₅
Molecular Weight:284.353
Hs Code.:

Synonyms:(2R,3R,4S)-2-(4-methoxybenzyl)oxymethyl-1,2,4-trihydroxyhexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R,4S)-2-(4-methoxybenzyl)oxymethyl-1,2,4-trihydroxyhexane

Chemical Property:

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Technology Process of (2R,3R,4S)-2-(4-methoxybenzyl)oxymethyl-1,2,4-trihydroxyhexane

There total 6 articles about (2R,3R,4S)-2-(4-methoxybenzyl)oxymethyl-1,2,4-trihydroxyhexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 113956-97-1
3-C-(4-methoxybenzyl)oxymethyl-3,5,6-trideoxy-α-D-ribo-hexofuranose

: 113956-98-2
(2R,3R,4S)-2-(4-methoxybenzyl)oxymethyl-1,2,4-trihydroxyhexane

Guidance literature:: With calcium borohydride; In ethanol; for 1h; Ambient temperature;
DOI:10.1248/cpb.35.2219

Reference yield:

: 98039-10-2
3-deoxy-1,2,5,6-di-O-isopropylidene-3-C-(4-metoxybenzyloxymethyl)-α-D-allofuranose

: 113956-98-2
(2R,3R,4S)-2-(4-methoxybenzyl)oxymethyl-1,2,4-trihydroxyhexane

Guidance literature:: Multi-step reaction with 6 steps

1: 86.5 percent / 2percent H₂SO₄ / methanol / 15 h / Ambient temperature

2: Et₃N/DMAP / CH₂Cl₂ / 19 h / Ambient temperature

3: NaI / butan-2-one / 24 h / Heating

4: 98.5 percent / H₂ / 10percent Pd-C / 0.5 h

5: 70 percent / 4.5 N HCl / tetrahydrofuran / 5.5 h / 50 °C

6: 86 percent / Ca(BH₄)2 / ethanol / 1 h / Ambient temperature

With hydrogenchloride; dmap; calcium borohydride; sulfuric acid; hydrogen; triethylamine; sodium iodide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; butanone;
DOI:10.1248/cpb.35.2219

Reference yield:

: 86654-47-9
(R)-1-[(3aR,5S,6R,6aR)-6-(4-Methoxy-benzyloxymethyl)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl]-ethane-1,2-diol

: 113956-98-2
(2R,3R,4S)-2-(4-methoxybenzyl)oxymethyl-1,2,4-trihydroxyhexane

Guidance literature:: Multi-step reaction with 5 steps

1: Et₃N/DMAP / CH₂Cl₂ / 19 h / Ambient temperature

2: NaI / butan-2-one / 24 h / Heating

3: 98.5 percent / H₂ / 10percent Pd-C / 0.5 h

4: 70 percent / 4.5 N HCl / tetrahydrofuran / 5.5 h / 50 °C

5: 86 percent / Ca(BH₄)2 / ethanol / 1 h / Ambient temperature

With hydrogenchloride; dmap; calcium borohydride; hydrogen; triethylamine; sodium iodide; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; butanone;
DOI:10.1248/cpb.35.2219