CH₃OC₆H₄C₁₂N₂H₆C₆H₂(C₆H₁₃)2C₁₂N₂H₆C₆H₄OCH₃

Base Information

• Chemical Name: CH₃OC₆H₄C₁₂N₂H₆C₆H₂(C₆H₁₃)2C₁₂N₂H₆C₆H₄OCH₃
• CAS No.: 256504-86-6
• Molecular Formula: C₅₆H₅₄N₄O₂
• Molecular Weight: 815.07
• Mol file: 256504-86-6.mol

Synonyms:CH₃OC₆H₄C₁₂N₂H₆C₆H₂(C₆H₁₃)2C₁₂N₂H₆C₆H₄OCH₃

Chemical Property of CH₃OC₆H₄C₁₂N₂H₆C₆H₂(C₆H₁₃)2C₁₂N₂H₆C₆H₄OCH₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of CH₃OC₆H₄C₁₂N₂H₆C₆H₂(C₆H₁₃)2C₁₂N₂H₆C₆H₄OCH₃

There total 3 articles about CH₃OC₆H₄C₁₂N₂H₆C₆H₂(C₆H₁₃)2C₁₂N₂H₆C₆H₄OCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

p-methoxyphenyllithium (14774-77-7) + C42H42N4 → CH3OC6H4C12N2H6C6H2(C6H13)2C12N2H6C6H4OCH3 (256504-86-6)

Guidance literature:

In tetrahydrofuran; at -5 ℃;

DOI:10.1039/a907284e

Reference yield:

3-bromophenanthroline (66127-01-3) → CH3OC6H4C12N2H6C6H2(C6H13)2C12N2H6C6H4OCH3 (256504-86-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 55 percent / Na₂CO₃; water / Pd(PPh₃)4 / ethanol; toluene / Heating

2: 32 percent / tetrahydrofuran / -5 °C

With water; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; toluene; 1: Substitution / 2: Arylation;

DOI:10.1039/a907284e

Reference yield:

2,5-dihexyl-1,4-phenylenediboronic acid (131117-66-3) → CH3OC6H4C12N2H6C6H2(C6H13)2C12N2H6C6H4OCH3 (256504-86-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 55 percent / Na₂CO₃; water / Pd(PPh₃)4 / ethanol; toluene / Heating

2: 32 percent / tetrahydrofuran / -5 °C

With water; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; toluene; 1: Substitution / 2: Arylation;

DOI:10.1039/a907284e

upstream raw materials:

p-methoxyphenyllithium

3-bromophenanthroline

2,5-dihexyl-1,4-phenylenediboronic acid

Refernces