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3-Bromo-1,10-phenanthroline is a chemical compound characterized by a phenanthroline ring with a bromine atom attached at the 3-position. This structural feature endows it with unique reactivity and solubility properties, making it a versatile agent in various analytical and synthetic applications.

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  • 66127-01-3 Structure
  • Basic information

    1. Product Name: 3-BROMO-1,10-PHENANTHROLINE
    2. Synonyms: 1,10-Phenanthroline,3-bromo-;3-BROMO-1,10-PHENTHROLINE;3-BROMO-1,10-PHENANTHROLINE;3-Bromophenanthroline
    3. CAS NO:66127-01-3
    4. Molecular Formula: C12H7BrN2
    5. Molecular Weight: 259.1
    6. EINECS: N/A
    7. Product Categories: Electronic Chemicals
    8. Mol File: 66127-01-3.mol
  • Chemical Properties

    1. Melting Point: 173 °C
    2. Boiling Point: 397.8 °C at 760 mmHg
    3. Flash Point: 194.4 °C
    4. Appearance: Yellow crystalline powder
    5. Density: 1.616
    6. Vapor Pressure: 3.55E-06mmHg at 25°C
    7. Refractive Index: 1.757
    8. Storage Temp.: Sealed in dry,Room Temperature
    9. Solubility: soluble in Methanol
    10. PKA: 4.22±0.10(Predicted)
    11. CAS DataBase Reference: 3-BROMO-1,10-PHENANTHROLINE(CAS DataBase Reference)
    12. NIST Chemistry Reference: 3-BROMO-1,10-PHENANTHROLINE(66127-01-3)
    13. EPA Substance Registry System: 3-BROMO-1,10-PHENANTHROLINE(66127-01-3)
  • Safety Data

    1. Hazard Codes: N/A
    2. Statements: N/A
    3. Safety Statements: 24/25
    4. WGK Germany:
    5. RTECS:
    6. HazardClass: N/A
    7. PackingGroup: N/A
    8. Hazardous Substances Data: 66127-01-3(Hazardous Substances Data)

66127-01-3 Usage

Uses

Used in Analytical Chemistry:
3-Bromo-1,10-phenanthroline serves as a chelating agent for transition metal ions, which is particularly useful in spectrophotometric and fluorometric analyses. Its ability to form complexes with metal ions allows for the detection and quantification of these ions in samples.
Used in Research Laboratories:
In research settings, 3-Bromo-1,10-phenanthroline is utilized as a fluorescent probe for the detection and quantification of metal ions in biological and environmental samples. The bromine atom's presence enhances its sensitivity and selectivity in these applications.
Used in the Synthesis of Coordination Complexes:
3-Bromo-1,10-phenanthroline is employed in the synthesis of coordination complexes, where its chelating properties are leveraged to create stable and functional molecular structures with potential applications in various fields, including catalysis and materials science.
Used in Catalytic Reactions:
Furthermore, 3-Bromo-1,10-phenanthroline has been investigated for its role in catalytic reactions, where its interaction with metal ions can facilitate or enhance the reaction processes, contributing to the development of more efficient and selective catalytic systems.

Check Digit Verification of cas no

The CAS Registry Mumber 66127-01-3 includes 8 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 5 digits, 6,6,1,2 and 7 respectively; the second part has 2 digits, 0 and 1 respectively.
Calculate Digit Verification of CAS Registry Number 66127-01:
(7*6)+(6*6)+(5*1)+(4*2)+(3*7)+(2*0)+(1*1)=113
113 % 10 = 3
So 66127-01-3 is a valid CAS Registry Number.
InChI:InChI=1/C12H7BrN2/c13-10-6-9-4-3-8-2-1-5-14-11(8)12(9)15-7-10/h1-7H

66127-01-3 Well-known Company Product Price

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  • TCI America

  • (B2632)  3-Bromo-1,10-phenanthroline  >98.0%(HPLC)(T)

  • 66127-01-3

  • 200mg

  • 1,750.00CNY

  • Detail

66127-01-3SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name 3-Bromo-1,10-phenanthroline

1.2 Other means of identification

Product number -
Other names 3-BROMO-1,10-PHENANTHROLINE

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:66127-01-3 SDS

66127-01-3Relevant articles and documents

Photobiological activity of Ru(ll) dyads based on (Pyren-1 -yl)ethynyl derivatives of 1, 10-Phenanthroline

Monro, Susan,Scott, John,Chouai, Abdellatif,Lincoln, Richard,Zong, Ruifa,Thummel, Randolph P.,McFarland, Sherri A.

body text, p. 2889 - 2900 (2010/05/15)

Several mononuclear Ru(ll) dyads possessing 1, 10-phenanthrollne-appended pyrenylethynylene llgands were synthesized, characterized, and evaluated for their potential in photobiologlcal applications such as photodynamlc therapy (PDT). These complexes interact with DNA via intercalation and photocleave DNA in vitro at submlcromolar concentrations when irradiated with visible light (λirr ≥ 400 nm). Such properties are remarkably sensitive to the position of the ethynylpyrenyl substituent on the 1, 10-phenanthroline ring, with 3-substitutlon showing the strongest binding under all conditions and causing the most deleterious DNA damage. Both dyads photocleave DNA under hypoxic conditions, and this photoactlvity translates well to cytotoxicity and photocytotoxlcity models using human leukemia cells, where the 5- and 3-substituted dyads show photocytotoxiclty at 5-10μM and 10-20μM, respectively, with minimal, or essentially no, dark toxicity at these concentrations. This lack of dark cytotoxicity at concentrations where significant photoactlvity Is observed emphasizes that agents with strong intercalating units, previously thought to be too toxic for phototherapeutic applications, should not be excluded from the arsenal of potential photochemotherapeutic agents under investigation.

Synthesis and properties of 3,8-bis[4-(9H-carbazol-9-yl)phenyl]-1,10- phenanthroline for phosphorescent OLEDs

Ge, Ziyi,Hayakawa, Teruaki,Ando, Shinji,Ueda, Mitsuru,Akiike, Toshiyuki,Miyamoto, Hidetoshi,Kajita, Toru,Kakimoto, Masa-aki

, p. 262 - 263 (2008/09/20)

A novel bipolar molecule, 3,8-bis[4-(9H-carbazol-9-yl)-phenyl]-1,10- phenanthroline (CZPT) was synthesized and employed as the host in phosphorescent organic light-emitting devices (OLEDs). A maximum luminance of 7000 cd/m 2 was achieved using fac-tris(2-phenylpyridine)iridium (Ir(ppy) 3) as the emitting material. Copyright

Liquid-crystalline phenanthrolines

Bousquet,Bruce

, p. 1769 - 1771 (2007/10/03)

The synthesis and mesomorphism of the first liquid-crystalline phenanthrolines are reported.

Simple One-Step Synthesis of 3-Bromo- and 3,8-Dibromo-1,10-Phenanthroline: Fundamental Building Blocks in the Design of Metal Chelates

Tzalis, Dimitrios,Tor, Yitzhak,Failla, Salvatorre,Siegel, Jay S.

, p. 3489 - 3490 (2007/10/02)

Commercially available 1,10-phenanthroline monohydrochloride monohydrate (1) reacts with bromine to give 3-bromo-1,10-phenanthroline (2) and 3,8-dibromo-1,10-phenanthroline (3) as major products in a one step reaction.

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