3,3'-[1,2-ethanediylbis[[[(1,1-dimethylethoxy)carbonyl]imino]-2,1-ethanediyliminocarbonothioyl-4,2-thiazolediyl]]-bis[4-hydroxy]benzoic acid dimethyl ester

Base Information

Chemical Name:3,3'-[1,2-ethanediylbis[[[(1,1-dimethylethoxy)carbonyl]imino]-2,1-ethanediyliminocarbonothioyl-4,2-thiazolediyl]]-bis[4-hydroxy]benzoic acid dimethyl ester
CAS No.:1148627-89-7
Molecular Formula:C₄₀H₄₈N₆O₁₀S₄
Molecular Weight:901.119
Hs Code.:

3,3'-[1,2-ethanediylbis[[[(1,1-dimethylethoxy)carbonyl]imino]-2,1-ethanediyliminocarbonothioyl-4,2-thiazolediyl]]-bis[4-hydroxy]benzoic acid dimethyl ester

Synonyms:3,3'-[1,2-ethanediylbis[[[(1,1-dimethylethoxy)carbonyl]imino]-2,1-ethanediyliminocarbonothioyl-4,2-thiazolediyl]]-bis[4-hydroxy]benzoic acid dimethyl ester

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Chemical Property of 3,3'-[1,2-ethanediylbis[[[(1,1-dimethylethoxy)carbonyl]imino]-2,1-ethanediyliminocarbonothioyl-4,2-thiazolediyl]]-bis[4-hydroxy]benzoic acid dimethyl ester

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Technology Process of 3,3'-[1,2-ethanediylbis[[[(1,1-dimethylethoxy)carbonyl]imino]-2,1-ethanediyliminocarbonothioyl-4,2-thiazolediyl]]-bis[4-hydroxy]benzoic acid dimethyl ester

There total 3 articles about 3,3'-[1,2-ethanediylbis[[[(1,1-dimethylethoxy)carbonyl]imino]-2,1-ethanediyliminocarbonothioyl-4,2-thiazolediyl]]-bis[4-hydroxy]benzoic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1148627-82-0
3,3'-[1,2-ethanediylbis[[[(1,1-dimethylethoxy)carbonyl]imino]-2,1-ethanediyliminocarbonyl-4,2-thiazolediyl]]-bis[4-hydroxy]benzoic acid dimethyl ester

: 1148627-89-7
3,3'-[1,2-ethanediylbis[[[(1,1-dimethylethoxy)carbonyl]imino]-2,1-ethanediyliminocarbonothioyl-4,2-thiazolediyl]]-bis[4-hydroxy]benzoic acid dimethyl ester

Guidance literature:: With Lawessons reagent; In toluene; for 3h; regioselective reaction; Reflux;
DOI:10.1016/j.tet.2011.01.008

Reference yield:

: 206531-21-7
tert-butyl N-(2-aminoethyl)-N-[2-(2-aminoethyl(tert-butoxycarbonyl)amino)ethyl]carbamate

: 1148627-89-7
3,3'-[1,2-ethanediylbis[[[(1,1-dimethylethoxy)carbonyl]imino]-2,1-ethanediyliminocarbonothioyl-4,2-thiazolediyl]]-bis[4-hydroxy]benzoic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 16 h / 20 °C / Inert atmosphere

2: Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 16 h / 0 - 25 °C / Inert atmosphere

3: Lawessons reagent / toluene / 3 h / Reflux

With Lawessons reagent; Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; toluene;
DOI:10.1016/j.tet.2011.01.008

Reference yield:

: 1148627-83-1
C₄₀H₅₂N₆O₁₂S₂

: 1148627-89-7
3,3'-[1,2-ethanediylbis[[[(1,1-dimethylethoxy)carbonyl]imino]-2,1-ethanediyliminocarbonothioyl-4,2-thiazolediyl]]-bis[4-hydroxy]benzoic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 16 h / 0 - 25 °C / Inert atmosphere

2: Lawessons reagent / toluene / 3 h / Reflux

With Lawessons reagent; Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; toluene;
DOI:10.1016/j.tet.2011.01.008