2-phenoxy acetic acid fluoride

Base Information

Chemical Name:2-phenoxy acetic acid fluoride
CAS No.:54705-70-3
Molecular Formula:C₈H₇FO₂
Molecular Weight:154.141
Hs Code.:

Synonyms:2-phenoxy acetic acid fluoride

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Chemical Property of 2-phenoxy acetic acid fluoride

Chemical Property:

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Technology Process of 2-phenoxy acetic acid fluoride

There total 2 articles about 2-phenoxy acetic acid fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 122-59-8
2-phenoxyacetic acid

: 54705-70-3
2-phenoxy acetic acid fluoride

Guidance literature:: With pyridine; trifluoro-[1,3,5]triazine; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1002/ejoc.201300389

Reference yield: 69.0%

: 701-99-5
Phenoxyacetyl chloride

: 54705-70-3
2-phenoxy acetic acid fluoride

Guidance literature:: With potassium hydrogenfluoride; tetrabutyl-ammonium chloride; water; In dichloromethane; at 20 ℃; for 0.333333h; Cooling with ice;
DOI:10.1055/a-1649-5460

Reference yield: 100.0%

: 54705-70-3
2-phenoxy acetic acid fluoride

: 220329-71-5
(S)-2-((E)-3-Pyrrolidin-1-yl-propenyl)-pyrrolidine-1-carboxylic acid tert-butyl ester

: (2S)-2[(1R)-1-[(1R)-2-oxo-1-phenoxy-2-(1-pyrrolidinyl)ethyl]-2-propen-1-yl]-1-pyrrolidinecarboxylic acid-tert-butyl ester

Guidance literature:: With trimethylaluminum; sodium carbonate; In dichloromethane; toluene; at 0 - 20 ℃; for 12h; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201300389