2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)-7-vinyl-4,5-dihydronaphtho[1,2-d]oxazole

Base Information

Chemical Name:2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)-7-vinyl-4,5-dihydronaphtho[1,2-d]oxazole
CAS No.:1307812-90-3
Molecular Formula:C₂₇H₂₈FNO
Molecular Weight:401.524
Hs Code.:

Synonyms:2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)-7-vinyl-4,5-dihydronaphtho[1,2-d]oxazole

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Chemical Property of 2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)-7-vinyl-4,5-dihydronaphtho[1,2-d]oxazole

Chemical Property:

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Technology Process of 2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)-7-vinyl-4,5-dihydronaphtho[1,2-d]oxazole

There total 9 articles about 2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)-7-vinyl-4,5-dihydronaphtho[1,2-d]oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1307812-05-0
6-vinyl-3,4-dihydronaphthalen-1(2H)-one oxime

: 1307815-63-9
3-(1-(4-fluorophenyl)cyclohexyl)propanoyl chloride

: 1307812-90-3
2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)-7-vinyl-4,5-dihydronaphtho[1,2-d]oxazole

Guidance literature:: With dmap; In 1,2-dichloro-benzene; at 180 ℃; for 0.166667h; Microwave irradiation;

Reference yield:

: 3470-50-6
6-Hydroxy-1-tetralone

: 1307812-90-3
2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)-7-vinyl-4,5-dihydronaphtho[1,2-d]oxazole

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 4 h / 0 - 20 °C

2: lithium chloride / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 14 h / 100 °C / Inert atmosphere

3: hydroxylamine hydrochloride; sodium acetate / methanol / 1.5 h / 80 °C

4: dmap / 1,2-dichloro-benzene / 0.17 h / 180 °C / Microwave irradiation

With pyridine; dmap; hydroxylamine hydrochloride; sodium acetate; lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; methanol; 1,2-dichloro-benzene;

Reference yield:

: 144464-64-2
5-oxo-5,6,7,8-tetrahydronaphthalen-2-yl trifluoromethanesulfonate

: 1307812-90-3
2-(2-(1-(4-fluorophenyl)cyclohexyl)ethyl)-7-vinyl-4,5-dihydronaphtho[1,2-d]oxazole

Guidance literature:: Multi-step reaction with 3 steps

1: lithium chloride / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 14 h / 100 °C / Inert atmosphere

2: hydroxylamine hydrochloride; sodium acetate / methanol / 1.5 h / 80 °C

3: dmap / 1,2-dichloro-benzene / 0.17 h / 180 °C / Microwave irradiation

With dmap; hydroxylamine hydrochloride; sodium acetate; lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; methanol; 1,2-dichloro-benzene;