N-(fluorenyl-9-methoxycarbonyl)-L-(p-sulfomethyl)phenylalanine methyl ester

Base Information

Chemical Name:N-(fluorenyl-9-methoxycarbonyl)-L-(p-sulfomethyl)phenylalanine methyl ester
CAS No.:945245-47-6
Molecular Formula:C₂₆H₂₅NO₇S
Molecular Weight:495.553
Hs Code.:

Synonyms:N-(fluorenyl-9-methoxycarbonyl)-L-(p-sulfomethyl)phenylalanine methyl ester

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Chemical Property of N-(fluorenyl-9-methoxycarbonyl)-L-(p-sulfomethyl)phenylalanine methyl ester

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of N-(fluorenyl-9-methoxycarbonyl)-L-(p-sulfomethyl)phenylalanine methyl ester

There total 9 articles about N-(fluorenyl-9-methoxycarbonyl)-L-(p-sulfomethyl)phenylalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 945245-46-5
N-(fluorenyl-9-methoxycarbonyl)-L-(p-bromomethyl)phenylalanine methyl ester

: 945245-47-6
N-(fluorenyl-9-methoxycarbonyl)-L-(p-sulfomethyl)phenylalanine methyl ester

Guidance literature:: With water; sodium sulfite; In 1,4-dioxane; at 100 ℃; for 1h;
DOI:10.1016/j.tet.2007.03.028

Reference yield:

: 298693-92-2
N-(fluorenyl-9-methoxycarbonyl)-L-O-trifluoromethylsulfonyl-tyrosine methyl ester

: 945245-47-6
N-(fluorenyl-9-methoxycarbonyl)-L-(p-sulfomethyl)phenylalanine methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,3-bis-(diphenylphosphino)-propane; triethylamine / Pd(OAc)2 / dimethylformamide / 0.17 h

1.2: 40 percent / trioctylsilane / dimethylformamide / 12 h / 70 °C

2.1: 72 percent / sodium borohydride / CH₂Cl₂; methanol / 0.67 h / 20 °C

3.1: 83 percent / triphenylphosphine; N-bromo-succinimide / tetrahydrofuran / 0 - 20 °C

4.1: 100 percent / sodium sulfite; H₂O / dioxane / 1 h / 100 °C

With sodium tetrahydroborate; N-Bromosuccinimide; water; triethylamine; triphenylphosphine; sodium sulfite; palladium diacetate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.03.028

Reference yield:

: 82911-79-3
N-(fluorenyl-9-methoxycarbonyl)-L-tyrosine methyl ester

: 945245-47-6
N-(fluorenyl-9-methoxycarbonyl)-L-(p-sulfomethyl)phenylalanine methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: 81 percent / pyridine / CH₂Cl₂ / 0.67 h / 0 - 5 °C

2.1: 1,3-bis-(diphenylphosphino)-propane; triethylamine / Pd(OAc)2 / dimethylformamide / 0.17 h

2.2: 40 percent / trioctylsilane / dimethylformamide / 12 h / 70 °C

3.1: 72 percent / sodium borohydride / CH₂Cl₂; methanol / 0.67 h / 20 °C

4.1: 83 percent / triphenylphosphine; N-bromo-succinimide / tetrahydrofuran / 0 - 20 °C

5.1: 100 percent / sodium sulfite; H₂O / dioxane / 1 h / 100 °C

With pyridine; sodium tetrahydroborate; N-Bromosuccinimide; water; triethylamine; triphenylphosphine; sodium sulfite; palladium diacetate; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.03.028