phenyltrinitromethane

Base Information

• Chemical Name: phenyltrinitromethane
• CAS No.: 67483-29-8
• Molecular Formula: C₇H₅N₃O₆
• Molecular Weight: 227.133

Synonyms:phenyltrinitromethane

Chemical Property of phenyltrinitromethane

Chemical Property:

Purity/Quality:

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Technology Process of phenyltrinitromethane

There total 14 articles about phenyltrinitromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

benzonitrile oxide (873-67-6) → 3,4-diphenyl-furazan 2-oxide (5585-14-8) + phenyltrinitromethane (67483-29-8) + benzonitrile (100-47-0)

Guidance literature:

With nitrogen(II) oxide; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1007/BF00957863

Reference yield: 37.0%

benzonitrile oxide (873-67-6) → 3,4-diphenyl-furazan 2-oxide (5585-14-8) + phenyltrinitromethane (67483-29-8)

Guidance literature:

With dinitrogen trioxide; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1007/BF00957863

Reference yield: 26.0%

benzonitrile oxide (873-67-6) → phenyltrinitromethane (67483-29-8) + benzoic acid (65-85-0,8013-63-6)

Guidance literature:

With dinitrogen tetraoxide; In dichloromethane; at 18 - 20 ℃; for 3h;

DOI:10.1007/BF00957862

upstream raw materials:

toluene

benzonitrile oxide

potassium trinitromethanide

potassium salt of phenyldinitromethane

Downstream raw materials:

m-nitrophenyltrinitromethane

3-{N-Methyl-N'-[1-nitro-1-phenyl-meth-(E)-ylidene]-hydrazino}-propionitrile

N,N-Dimethyl-N'-[1-nitro-1-phenyl-meth-(E)-ylidene]-hydrazine

Dinitromethyl-benzene; compound with methyl-hydrazine

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