C₂₉H₄₀O₆Si

Base Information

Chemical Name:C₂₉H₄₀O₆Si
CAS No.:1032880-02-6
Molecular Formula:C₂₉H₄₀O₆Si
Molecular Weight:512.718
Hs Code.:

C<sub>29</sub>H<sub>40</sub>O<sub>6</sub>Si

Synonyms:C₂₉H₄₀O₆Si

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Chemical Property of C₂₉H₄₀O₆Si

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Technology Process of C₂₉H₄₀O₆Si

There total 10 articles about C₂₉H₄₀O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1032880-00-4
C₂₄H₃₂O₅Si

: 3282-30-2
pivaloyl chloride

: 1032880-02-6
C₂₉H₄₀O₆Si

Guidance literature:: With pyridine; dmap; In dichloromethane; at 20 ℃;
DOI:10.1021/ol8008057

Reference yield:

: 1032879-81-4
C₂₇H₃₈O₄Si

: 1032880-02-6
C₂₉H₄₀O₆Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 5 h / 0 - 20 °C

1.2: 2 h / Reflux

2.1: dimethyl sulfoxide; triethylamine; sulfur trioxide pyridine complex / dichloromethane / 2 h / -10 °C

3.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol / 1 h / -10 - 20 °C

4.1: toluene-4-sulfonic acid / dichloromethane / 3 h / 0 - 20 °C

5.1: pyridine; dmap / dichloromethane / 20 °C

With pyridine; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; sulfur trioxide pyridine complex; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.3987/COM-12-S(N)54

Reference yield:

: 101331-92-4
4-O-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-L-threose

: 1032880-02-6
C₂₉H₄₀O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: (-)-B-methoxydiisopinocamphenylborane / diethyl ether / 1 h / 0 - 20 °C

1.2: 3 h / -78 °C

2.1: sodium hydride / tetrahydrofuran / 1 h / -10 - 20 °C

2.2: 12 h / 20 °C

3.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 5 h / 0 - 20 °C

3.2: 2 h / Reflux

4.1: dimethyl sulfoxide; triethylamine; sulfur trioxide pyridine complex / dichloromethane / 2 h / -10 °C

5.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol / 1 h / -10 - 20 °C

6.1: toluene-4-sulfonic acid / dichloromethane / 3 h / 0 - 20 °C

7.1: pyridine; dmap / dichloromethane / 20 °C

With pyridine; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; (-)-B-methoxydiisopinocamphenylborane; sulfur trioxide pyridine complex; sodium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; diethyl ether; dichloromethane; water; tert-butyl alcohol;
DOI:10.3987/COM-12-S(N)54