[2-benzenesulfonylmethyl-4-(pentafluorosulfanyl)phenyl]-(4-chlorobenzylidine)-amine

Base Information

Chemical Name:[2-benzenesulfonylmethyl-4-(pentafluorosulfanyl)phenyl]-(4-chlorobenzylidine)-amine
CAS No.:1446250-11-8
Molecular Formula:C₂₀H₁₅ClF₅NO₂S₂
Molecular Weight:495.922
Hs Code.:

Synonyms:[2-benzenesulfonylmethyl-4-(pentafluorosulfanyl)phenyl]-(4-chlorobenzylidine)-amine

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Chemical Property of [2-benzenesulfonylmethyl-4-(pentafluorosulfanyl)phenyl]-(4-chlorobenzylidine)-amine

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Technology Process of [2-benzenesulfonylmethyl-4-(pentafluorosulfanyl)phenyl]-(4-chlorobenzylidine)-amine

There total 4 articles about [2-benzenesulfonylmethyl-4-(pentafluorosulfanyl)phenyl]-(4-chlorobenzylidine)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1446250-10-7
4-(pentafluoro-λ⁶-sulfanyl)-2-((phenylsulfonyl)methyl)aniline

: 104-88-1
4-chlorobenzaldehyde

: 1446250-11-8
[2-benzenesulfonylmethyl-4-(pentafluorosulfanyl)phenyl]-(4-chlorobenzylidine)-amine

Guidance literature:: With magnesium sulfate; acetic acid; at 60 - 70 ℃; for 2h; Inert atmosphere;
DOI:10.1055/s-0032-1318452

Reference yield:

: 2613-27-6
1-nitro-4-(pentafluorosulfanyl)benzene

: 1446250-11-8
[2-benzenesulfonylmethyl-4-(pentafluorosulfanyl)phenyl]-(4-chlorobenzylidine)-amine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium tert-butylate / N,N-dimethyl-formamide / 0.5 h / -40 °C

2: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / 750.08 Torr

3: acetic acid; magnesium sulfate / 2 h / 60 - 70 °C / Inert atmosphere

With palladium 10% on activated carbon; potassium tert-butylate; hydrogen; magnesium sulfate; acetic acid; In ethanol; N,N-dimethyl-formamide;
DOI:10.1055/s-0032-1318452

Reference yield:

: 7205-98-3
chloromethyl phenyl sulfone

: 1446250-11-8
[2-benzenesulfonylmethyl-4-(pentafluorosulfanyl)phenyl]-(4-chlorobenzylidine)-amine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium tert-butylate / N,N-dimethyl-formamide / 0.5 h / -40 °C

2: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / 750.08 Torr

3: acetic acid; magnesium sulfate / 2 h / 60 - 70 °C / Inert atmosphere

With palladium 10% on activated carbon; potassium tert-butylate; hydrogen; magnesium sulfate; acetic acid; In ethanol; N,N-dimethyl-formamide;
DOI:10.1055/s-0032-1318452