4-Decylpyridine

Base Information

• Chemical Name: 4-Decylpyridine
• CAS No.: 1815-99-2
• Molecular Formula: C₁₅H₂₅N
• Molecular Weight: 219.37
• Hs Code.: 2933399090
• European Community (EC) Number: 700-209-3
• DSSTox Substance ID: DTXSID4074643
• Nikkaji Number: J2.589.395F
• Wikidata: Q82002899
• Mol file: 1815-99-2.mol

Synonyms:4-Decylpyridine;1815-99-2;Pyridine, 4-decyl-;4-n-decylpyridine;SCHEMBL1261833;DTXSID4074643;YHYRSCXMQFIFNC-UHFFFAOYSA-N;BAA81599;MFCD00068592;AKOS016011888;DS-6987;CS-0152247;C73493;A880984

Chemical Property of 4-Decylpyridine

Chemical Property:

• PSA: 12.89000
• LogP: 4.76480
• Storage Temp.: Inert atmosphere,Room Temperature
• XLogP3: 5.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 9
• Exact Mass: 219.198699802
• Heavy Atom Count: 16
• Complexity: 138

Purity/Quality:

97% ^*data from raw suppliers

4-Decylpyridine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCC1=CC=NC=C1

Technology Process of 4-Decylpyridine

There total 4 articles about 4-Decylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

4-methoxypyridine (620-08-6,1232006-56-2) + decyl magnesium (1+); iodide → 4-decylpyridine (1815-99-2)

Guidance literature:

With bis(1,5-cyclooctadiene)nickel⁽⁰⁾; 1,2-bis-(dicyclohexylphosphino)ethane; In toluene; at 100 ℃; for 14h; Inert atmosphere; Glovebox; Sealed tube;

DOI:10.1021/jacs.6b03253

Reference yield:

picoline (108-89-4) → 4-decylpyridine (1815-99-2)

Guidance literature:

With diethyl ether; lithium diethylamide; anschliessendes Behandeln mit Nonylbromid;

Reference yield:

pyridinium p-toluenesulfonate (24057-28-1) → 2-decylpyridine (74421-02-6) + 4-decylpyridine (1815-99-2)

Guidance literature:

With C₁₀H₂₁Co(III)(dimethylglyoxime monoanion)2pyridine; In ethanol; for 24h; Product distribution; Mechanism; Irradiation; other heteroaromatic p-toluenosufonyl salts, and alkyl cobalt oximes; var. conditions of reaction;

DOI:10.1021/jo00254a058

upstream raw materials:

picoline

pyridinium p-toluenesulfonate

4-methoxypyridine