6-[(4-Acetyl-3-hydroxy-2-propylphenyl)methoxy]-1,2,3,4-tetrahydro-1-oxo-2-naphthaleneacetic acid

Base Information

Chemical Name:6-[(4-Acetyl-3-hydroxy-2-propylphenyl)methoxy]-1,2,3,4-tetrahydro-1-oxo-2-naphthaleneacetic acid
CAS No.:119348-58-2
Molecular Formula:C₂₄H₂₆O₆
Molecular Weight:410.467
Hs Code.:

Synonyms:6-[(4-Acetyl-3-hydroxy-2-propylphenyl)methoxy]-1,2,3,4-tetrahydro-1-oxo-2-naphthaleneacetic acid

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Chemical Property of 6-[(4-Acetyl-3-hydroxy-2-propylphenyl)methoxy]-1,2,3,4-tetrahydro-1-oxo-2-naphthaleneacetic acid

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Technology Process of 6-[(4-Acetyl-3-hydroxy-2-propylphenyl)methoxy]-1,2,3,4-tetrahydro-1-oxo-2-naphthaleneacetic acid

There total 5 articles about 6-[(4-Acetyl-3-hydroxy-2-propylphenyl)methoxy]-1,2,3,4-tetrahydro-1-oxo-2-naphthaleneacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 119348-56-0
6-[(4-acetyl-3-hydroxy-2-propylphenyl)methoxy]-1,2,3,4-tetrahydro-1-oxo-2-naphthaleneacetic acid, ethyl ester

: 119348-58-2
6-[(4-Acetyl-3-hydroxy-2-propylphenyl)methoxy]-1,2,3,4-tetrahydro-1-oxo-2-naphthaleneacetic acid

Guidance literature:: With sodium hydroxide; In ethanol; for 2h; Heating;
DOI:10.1021/jm00113a014

Reference yield: 43.0%

: 119348-58-2
6-[(4-Acetyl-3-hydroxy-2-propylphenyl)methoxy]-1,2,3,4-tetrahydro-1-oxo-2-naphthaleneacetic acid

Guidance literature:

Reference yield:

: 50558-96-8
6-methoxy-1,2,3,4-tetrahydro-1-oxonaphthalene-2-acetic acid, ethyl ester

: 119348-58-2
6-[(4-Acetyl-3-hydroxy-2-propylphenyl)methoxy]-1,2,3,4-tetrahydro-1-oxo-2-naphthaleneacetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 33 percent / AlCl₃ / CH₂Cl₂ / 20 h / Heating

2: 76 percent / potassium t-butoxide, NaI / ethanol / 30 h / Ambient temperature

3: 44 percent / 5 N NaOH / ethanol / 2 h / Heating

With sodium hydroxide; aluminium trichloride; potassium tert-butylate; sodium iodide; In ethanol; dichloromethane;
DOI:10.1021/jm00113a014