4-Benzyloxy-2-iodo-5-methoxybenzaldehyde

Base Information

Chemical Name:4-Benzyloxy-2-iodo-5-methoxybenzaldehyde
CAS No.:82583-97-9
Molecular Formula:C₁₅H₁₃IO₃
Molecular Weight:368.171
Hs Code.:
DSSTox Substance ID:DTXSID60509509
Wikidata:Q82367131

Synonyms:4-Benzyloxy-2-iodo-5-methoxybenzaldehyde;82583-97-9;SCHEMBL1617020;DTXSID60509509;HSDVAQOAWAQCRG-UHFFFAOYSA-N;4-(Benzyloxy)-2-iodo-5-methoxybenzaldehyde

Suppliers and Price of 4-Benzyloxy-2-iodo-5-methoxybenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 4-Benzyloxy-2-iodo-5-methoxybenzaldehyde

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:367.99094
Heavy Atom Count:19
Complexity:279

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C(=C1)C=O)I)OCC2=CC=CC=C2

Technology Process of 4-Benzyloxy-2-iodo-5-methoxybenzaldehyde

There total 7 articles about 4-Benzyloxy-2-iodo-5-methoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 82583-96-8
4-Benzyloxy-5-hydroxy-2-iodo-benzaldehyde

: 77-78-1
dimethyl sulfate

: 82583-97-9
4-benzyloxy-6-iodo-3-methoxybenzaldehyde

Guidance literature:: With sodium hydroxide; at 85 ℃; for 1h;

Reference yield:

: 712-97-0
6-nitro-1,3-benzodioxole-5-carbaldehyde

: 82583-97-9
4-benzyloxy-6-iodo-3-methoxybenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / methanol; dimethylsulfoxide; dimethylformamide / 2 h / 150 °C

2: 90 percent / K₂CO₃ / dimethylformamide / 2 h / 100 °C

3: 1.) FeSO₄ x 7 H₂O; 25 percent NH₄OH; 2.) 10 percent H₂SO₄; NaNO₂; KI / 2.) CuI / 1.) 5 min, 100 deg C 2.) AcOH, H₂O

With ammonium hydroxide; sulfuric acid; potassium carbonate; potassium iodide; sodium nitrite; copper(l) iodide; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 20194-18-7
sodium phenyl-methanolate

: 82583-97-9
4-benzyloxy-6-iodo-3-methoxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 14 percent / phenylmethanol; dimethylsulfoxide / 0.03 h / 180 °C

2: 94 percent / 2 percent NaOH / 1 h / 85 °C

With sodium hydroxide; In dimethyl sulfoxide; benzyl alcohol;