Technology Process of 4-Benzyloxy-2-iodo-5-methoxybenzaldehyde
There total 7 articles about 4-Benzyloxy-2-iodo-5-methoxybenzaldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
at 85 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 72 percent / methanol; dimethylsulfoxide; dimethylformamide / 2 h / 150 °C
2: 90 percent / K2CO3 / dimethylformamide / 2 h / 100 °C
3: 1.) FeSO4 x 7 H2O; 25 percent NH4OH; 2.) 10 percent H2SO4; NaNO2; KI / 2.) CuI / 1.) 5 min, 100 deg C 2.) AcOH, H2O
With
ammonium hydroxide; sulfuric acid; potassium carbonate; potassium iodide; sodium nitrite;
copper(l) iodide;
In
methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 14 percent / phenylmethanol; dimethylsulfoxide / 0.03 h / 180 °C
2: 94 percent / 2 percent NaOH / 1 h / 85 °C
With
sodium hydroxide;
In
dimethyl sulfoxide; benzyl alcohol;
