N-(1,2,2,2-tetrafluoro-1-phenylethyl)-S,S-difluorosulfilimine

Base Information

• Chemical Name: N-(1,2,2,2-tetrafluoro-1-phenylethyl)-S,S-difluorosulfilimine
• CAS No.: 80369-17-1
• Molecular Formula: C₈H₅F₆NS
• Molecular Weight: 261.191
• Mol file: 80369-17-1.mol

Synonyms:N-(1,2,2,2-tetrafluoro-1-phenylethyl)-S,S-difluorosulfilimine

Chemical Property of N-(1,2,2,2-tetrafluoro-1-phenylethyl)-S,S-difluorosulfilimine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(1,2,2,2-tetrafluoro-1-phenylethyl)-S,S-difluorosulfilimine

There total 2 articles about N-(1,2,2,2-tetrafluoro-1-phenylethyl)-S,S-difluorosulfilimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

1,1,1-trimethyl-N-(2,2,2-trifluoro-1-phenylethylidene)silanamine (80369-15-9) → trimethylsilyl fluoride (420-56-4) + N-(1,2,2,2-tetrafluoro-1-phenylethyl)-S,S-difluorosulfilimine (80369-17-1)

Guidance literature:

With sulfur tetrafluoride; autoclave;

Reference yield:

1-phenyl-2,2,2-trifluoroethylideneimine (45988-04-3,84452-45-9,84452-46-0) → N-(1,2,2,2-tetrafluoro-1-phenylethyl)-S,S-difluorosulfilimine (80369-17-1)

Guidance literature:

Multi-step reaction with 2 steps

1: butyllithium / ether, 2 h

2: 65 percent / SF₄ / autoclave

With n-butyllithium; sulfur tetrafluoride;

upstream raw materials:

1,1,1-trimethyl-N-(2,2,2-trifluoro-1-phenylethylidene)silanamine

1-phenyl-2,2,2-trifluoroethylideneimine