prop-2-ynyl 4-O-benzyl-2,3-dideoxy-6-O-[(1,1-dimethylethyl)dimethylsilyl]-α-D-erythro-hex-2-enopyranoside

Base Information

Chemical Name:prop-2-ynyl 4-O-benzyl-2,3-dideoxy-6-O-[(1,1-dimethylethyl)dimethylsilyl]-α-D-erythro-hex-2-enopyranoside
CAS No.:389620-56-8
Molecular Formula:C₂₂H₃₂O₄Si
Molecular Weight:388.579
Hs Code.:

Synonyms:prop-2-ynyl 4-O-benzyl-2,3-dideoxy-6-O-[(1,1-dimethylethyl)dimethylsilyl]-α-D-erythro-hex-2-enopyranoside

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Chemical Property of prop-2-ynyl 4-O-benzyl-2,3-dideoxy-6-O-[(1,1-dimethylethyl)dimethylsilyl]-α-D-erythro-hex-2-enopyranoside

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Technology Process of prop-2-ynyl 4-O-benzyl-2,3-dideoxy-6-O-[(1,1-dimethylethyl)dimethylsilyl]-α-D-erythro-hex-2-enopyranoside

There total 3 articles about prop-2-ynyl 4-O-benzyl-2,3-dideoxy-6-O-[(1,1-dimethylethyl)dimethylsilyl]-α-D-erythro-hex-2-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 98-88-4
benzoyl chloride

: 289494-54-8
prop-2-ynyl 2,3-dideoxy-6-O-[(1,1-dimethylethyl)dimethylsilyl]-α-D-erythro-hex-2-enopyranoside

: 389620-56-8
prop-2-ynyl 4-O-benzyl-2,3-dideoxy-6-O-[(1,1-dimethylethyl)dimethylsilyl]-α-D-erythro-hex-2-enopyranoside

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.1016/S0008-6215(01)00211-7

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 389620-56-8
prop-2-ynyl 4-O-benzyl-2,3-dideoxy-6-O-[(1,1-dimethylethyl)dimethylsilyl]-α-D-erythro-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / imidazole; 4-dimethylaminopyridine / CH₂Cl₂ / 8 h / 0 - 20 °C

2: 98 percent / pyridine / 20 °C

With pyridine; 1H-imidazole; dmap; In dichloromethane;
DOI:10.1016/S0008-6215(01)00211-7

Reference yield:

: 188605-67-6
(1-prop-2-ynyl)-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

: 389620-56-8
prop-2-ynyl 4-O-benzyl-2,3-dideoxy-6-O-[(1,1-dimethylethyl)dimethylsilyl]-α-D-erythro-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / imidazole; 4-dimethylaminopyridine / CH₂Cl₂ / 8 h / 0 - 20 °C

2: 98 percent / pyridine / 20 °C

With pyridine; 1H-imidazole; dmap; In dichloromethane;
DOI:10.1016/S0008-6215(01)00211-7