4,6-bis[N-(2-pyridylmethyl)-N-(2-(2-pyridyl)ethyl)aminomethyl]-2-phenylpyrimidine

Base Information

• Chemical Name: 4,6-bis[N-(2-pyridylmethyl)-N-(2-(2-pyridyl)ethyl)aminomethyl]-2-phenylpyrimidine
• CAS No.: 1392139-14-8
• Molecular Formula: C₃₈H₃₈N₈
• Molecular Weight: 606.773

Synonyms:4,6-bis[N-(2-pyridylmethyl)-N-(2-(2-pyridyl)ethyl)aminomethyl]-2-phenylpyrimidine

Chemical Property of 4,6-bis[N-(2-pyridylmethyl)-N-(2-(2-pyridyl)ethyl)aminomethyl]-2-phenylpyrimidine

Chemical Property:

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Technology Process of 4,6-bis[N-(2-pyridylmethyl)-N-(2-(2-pyridyl)ethyl)aminomethyl]-2-phenylpyrimidine

There total 1 articles about 4,6-bis[N-(2-pyridylmethyl)-N-(2-(2-pyridyl)ethyl)aminomethyl]-2-phenylpyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

4,6-bis(chloromethyl)-2-phenylpyrimidine (131291-66-2) + (2-pyridin-2-yl-ethyl)-pyridin-2-ylmethyl-amine (15395-61-6) → 4,6-bis[N-(2-pyridylmethyl)-N-(2-(2-pyridyl)ethyl)aminomethyl]-2-phenylpyrimidine (1392139-14-8)

Guidance literature:

With sodium carbonate; potassium iodide; In acetonitrile; Reflux;

DOI:10.1021/ic3012052 DOI:10.1021/ic3012052

Reference yield: 90.0%

[FeII(pyridine)4(NCBH3)2] + 4,6-bis[N-(2-pyridylmethyl)-N-(2-(2-pyridyl)ethyl)aminomethyl]-2-phenylpyrimidine (1392139-14-8) + water (7732-18-5) → C42H50B4Fe2N12*1.5H2O

Guidance literature:

In acetonitrile; for 2.16667h; Inert atmosphere; Reflux;

DOI:10.1021/ic3012052 DOI:10.1021/ic3012052

Reference yield: 79.0%

[FeII(pyridine)4(NCSe)2] (24835-36-7,15154-80-0) + 4,6-bis[N-(2-pyridylmethyl)-N-(2-(2-pyridyl)ethyl)aminomethyl]-2-phenylpyrimidine (1392139-14-8) + water (7732-18-5) → C42H38Fe2N12Se4*1.5H2O

Guidance literature:

In methanol; for 1h; Inert atmosphere; Reflux;

DOI:10.1021/ic3012052 DOI:10.1021/ic3012052

upstream raw materials:

4,6-bis(chloromethyl)-2-phenylpyrimidine

(2-pyridin-2-yl-ethyl)-pyridin-2-ylmethyl-amine

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