(Z)-(5-ethoxycarbonylmethyl-4-oxothiazolidin-2-ylidene)-1-phenylethanone

Base Information

• Chemical Name: (Z)-(5-ethoxycarbonylmethyl-4-oxothiazolidin-2-ylidene)-1-phenylethanone
• CAS No.: 204690-23-3
• Molecular Formula: C₁₅H₁₅NO₄S
• Molecular Weight: 305.354

Synonyms:(Z)-(5-ethoxycarbonylmethyl-4-oxothiazolidin-2-ylidene)-1-phenylethanone

Chemical Property of (Z)-(5-ethoxycarbonylmethyl-4-oxothiazolidin-2-ylidene)-1-phenylethanone

Chemical Property:

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Technology Process of (Z)-(5-ethoxycarbonylmethyl-4-oxothiazolidin-2-ylidene)-1-phenylethanone

There total 1 articles about (Z)-(5-ethoxycarbonylmethyl-4-oxothiazolidin-2-ylidene)-1-phenylethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

diethyl 2-mercaptosuccinate (23060-14-2) + Benzoylacetonitrile (614-16-4) → (Z)-(5-ethoxycarbonylmethyl-4-oxothiazolidin-2-ylidene)-1-phenylethanone (204690-23-3)

Guidance literature:

With potassium carbonate; In ethanol; for 7h; Heating;

DOI:10.1016/S0040-4020(03)01146-3

Reference yield: 93.0%

benzyl bromide (100-39-0) + (Z)-(5-ethoxycarbonylmethyl-4-oxothiazolidin-2-ylidene)-1-phenylethanone (204690-23-3) → (Z)-(3-benzyl-5-ethoxycarbonylmethyl-4-oxothiazolidin-2-ylidene)-1-phenylethanone (1354223-08-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

DOI:10.1016/j.tet.2013.05.087

Reference yield: 92.0%

(Z)-(5-ethoxycarbonylmethyl-4-oxothiazolidin-2-ylidene)-1-phenylethanone (204690-23-3) → ethyl 3-(5-phenyl-3H-1,2-dithiol-3-ylidenethiocarbamoyl)propanoate (615552-87-9)

Guidance literature:

With Lawessons reagent; In toluene; at 90 - 95 ℃; for 1h;

DOI:10.1016/S0040-4039(03)01721-0

upstream raw materials:

diethyl 2-mercaptosuccinate

Benzoylacetonitrile

Downstream raw materials:

(Z)-2-bromo-2-(5-ethoxycarbonylmethyl-4-oxothiazolidin-2-ylidene)-1-phenylethanone

(2E,5Z)-(5-ethoxycarbonylmethylidene-4-oxothiazolidine-2-ylidene)-1-phenylethanone

ethyl 3-(5-phenyl-3H-1,2-dithiol-3-ylidenethiocarbamoyl)propanoate

ethyl 4-oxo-(5-phenyl-3H-1,2-dithiol-3-ylideneamino)butanoate

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