1-Methyl-3-methylenepiperidin-2-one

Base Information

Chemical Name:1-Methyl-3-methylenepiperidin-2-one
CAS No.:1690-73-9
Molecular Formula:C7H11 N O
Molecular Weight:125.17
Hs Code.:
DSSTox Substance ID:DTXSID70440616
Nikkaji Number:J775.892H
Wikidata:Q82256971
Mol file:1690-73-9.mol

Synonyms:1-methyl-3-methylenepiperidin-2-one;1-methyl-3-methylidenepiperidin-2-one;1690-73-9;1-methyl-3-methylene-2-piperidinone;SCHEMBL762771;DTXSID70440616;AKOS015904957;CS-0244047;EN300-27130

Suppliers and Price of 1-Methyl-3-methylenepiperidin-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-methyl-3-methylidenepiperidin-2-one
50mg
$ 155.00

American Custom Chemicals Corporation
1-METHYL-3-METHYLENEPIPERIDIN-2-ONE 95.00%
5G
$ 1928.08

American Custom Chemicals Corporation
1-METHYL-3-METHYLENEPIPERIDIN-2-ONE 95.00%
2.5G
$ 1473.14

American Custom Chemicals Corporation
1-METHYL-3-METHYLENEPIPERIDIN-2-ONE 95.00%
1G
$ 983.52

Total 7 raw suppliers

Chemical Property of 1-Methyl-3-methylenepiperidin-2-one

Chemical Property:

PSA：20.31000
LogP:0.73270
XLogP3:0.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:125.084063974
Heavy Atom Count:9
Complexity:151

Purity/Quality:

99% ^*data from raw suppliers

1-methyl-3-methylidenepiperidin-2-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1CCCC(=C)C1=O

Technology Process of 1-Methyl-3-methylenepiperidin-2-one

There total 6 articles about 1-Methyl-3-methylenepiperidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: N-methyl-N-(1-phenylethyl)-N-(4-pentynyl)amine

: 201230-82-2
carbon monoxide

: 1690-73-9
1-methyl-3-methylenepiperidine-2-one

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; at 90 ℃; for 4h; under 70680 Torr;
DOI:10.1021/ol070080c

Reference yield: 59.0%

: 944276-44-2
3-(hydroxymethyl)-1-methylpiperidine-2-one

: 1690-73-9
1-methyl-3-methylenepiperidine-2-one

Guidance literature:: With copper(l) iodide; dicyclohexyl-carbodiimide; In toluene; for 1.16667h; Heating;
DOI:10.1002/ejoc.200601034

Reference yield: 45.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 931-20-4
1-methylpiperidin-2-one

: 1690-73-9
1-methyl-3-methylenepiperidine-2-one

Guidance literature:: 1-methylpiperidin-2-one; With sodium hydride; oxalic acid diethyl ester; In diethyl ether; at 35 - 40 ℃; for 72h;

formaldehyd; In xylene; at 100 ℃; for 1.5h; Further stages.;
DOI:10.1039/b000129p