N-(5-nitropyridin-2-ylmethyl)-N-pyridin-2-ylmethylbenzamide

Base Information

Chemical Name:N-(5-nitropyridin-2-ylmethyl)-N-pyridin-2-ylmethylbenzamide
CAS No.:1402045-96-8
Molecular Formula:C₁₉H₁₆N₄O₃
Molecular Weight:348.361
Hs Code.:

Synonyms:N-(5-nitropyridin-2-ylmethyl)-N-pyridin-2-ylmethylbenzamide

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Chemical Property of N-(5-nitropyridin-2-ylmethyl)-N-pyridin-2-ylmethylbenzamide

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Technology Process of N-(5-nitropyridin-2-ylmethyl)-N-pyridin-2-ylmethylbenzamide

There total 6 articles about N-(5-nitropyridin-2-ylmethyl)-N-pyridin-2-ylmethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1402046-08-5
(5-nitropyridine-2-ylmethyl)pyridin-2-ylmethylamine

: 98-88-4
benzoyl chloride

: 1402045-96-8
N-(5-nitropyridin-2-ylmethyl)-N-pyridin-2-ylmethylbenzamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jo301349t

Reference yield:

: 21203-68-9
2-methyl-5-nitropyridine

: 1402045-96-8
N-(5-nitropyridin-2-ylmethyl)-N-pyridin-2-ylmethylbenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: iodine; tert-Butyl iodide; trifluoroacetic acid / dimethyl sulfoxide / 3 h / 170 °C

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 3.5 h / 20 °C / Inert atmosphere

3: triethylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

With iodine; sodium tris(acetoxy)borohydride; tert-Butyl iodide; triethylamine; trifluoroacetic acid; In dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1021/jo301349t

Reference yield:

: 35969-75-6
5-nitro-2-pyridinecarbaldehyde

: 1402045-96-8
N-(5-nitropyridin-2-ylmethyl)-N-pyridin-2-ylmethylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 3.5 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

With sodium tris(acetoxy)borohydride; triethylamine; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jo301349t