Technology Process of C24H23NO4
There total 8 articles about C24H23NO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C16H15NO3;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
for 0.0833333h;
p-methoxybenzyl chloride;
In
N,N-dimethyl-formamide; mineral oil;
at 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / mineral oil; ethanol; diethyl ether / 0 - 20 °C
2.1: sodium acetate / methanol; water
2.2: 1 h / 0 °C
3.1: formic acid / 10 h / 100 °C
4.1: methanol / 1 h / 20 °C
5.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.08 h
5.2: 3 h / 20 °C
With
formic acid; sodium acetate; sodium hydride;
In
methanol; diethyl ether; ethanol; water; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: palladium diacetate / diethyl ether / 0 °C
2.1: hydrogenchloride / water; tetrahydrofuran / 4 h / 20 °C
3.1: sodium hydride / mineral oil; ethanol; diethyl ether / 0 - 20 °C
4.1: sodium acetate / methanol; water
4.2: 1 h / 0 °C
5.1: formic acid / 10 h / 100 °C
6.1: methanol / 1 h / 20 °C
7.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.08 h
7.2: 3 h / 20 °C
With
hydrogenchloride; formic acid; sodium acetate; palladium diacetate; sodium hydride;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; water; N,N-dimethyl-formamide; mineral oil;