1,1-dimethylethyl {3-[4-(propyloxy)-2-(trifluoromethyl)phenyl]-5-isoxazolyl}acetate

Base Information

Chemical Name:1,1-dimethylethyl {3-[4-(propyloxy)-2-(trifluoromethyl)phenyl]-5-isoxazolyl}acetate
CAS No.:1268385-39-2
Molecular Formula:C₁₉H₂₂F₃NO₄
Molecular Weight:385.383
Hs Code.:

Synonyms:1,1-dimethylethyl {3-[4-(propyloxy)-2-(trifluoromethyl)phenyl]-5-isoxazolyl}acetate

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Chemical Property of 1,1-dimethylethyl {3-[4-(propyloxy)-2-(trifluoromethyl)phenyl]-5-isoxazolyl}acetate

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Technology Process of 1,1-dimethylethyl {3-[4-(propyloxy)-2-(trifluoromethyl)phenyl]-5-isoxazolyl}acetate

There total 4 articles about 1,1-dimethylethyl {3-[4-(propyloxy)-2-(trifluoromethyl)phenyl]-5-isoxazolyl}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1268385-33-6
{3-[4-(propyloxy)-2-(trifluoromethyl)phenyl]-5-isoxazolyl}-acetic Acid

: 115-11-7,15220-85-6
isobutene

: 1268385-39-2
1,1-dimethylethyl {3-[4-(propyloxy)-2-(trifluoromethyl)phenyl]-5-isoxazolyl}acetate

Guidance literature:: With sulfuric acid; In diethyl ether; water; isopropyl alcohol; at 20 ℃; Cooling with dry ice;

Reference yield:

: 1234790-81-8
4-(propyloxy)-2-(trifluoromethyl)benzaldehyde

: 1268385-39-2
1,1-dimethylethyl {3-[4-(propyloxy)-2-(trifluoromethyl)phenyl]-5-isoxazolyl}acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydroxylamine / ethanol; water / 2 h / 20 °C

2.1: N-chloro-succinimide / N,N-dimethyl-formamide / 0 °C

2.2: Reflux

3.1: periodic acid / acetonitrile / 0 - 20 °C

3.2: 0 - 20 °C

4.1: sulfuric acid / isopropyl alcohol; diethyl ether; water / 20 °C / Cooling with dry ice

With N-chloro-succinimide; sulfuric acid; hydroxylamine; periodic acid; In diethyl ether; ethanol; water; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;

Reference yield:

: 1268385-32-5
2-{3-[4-(propyloxy)-2-(trifluoromethyl)phenyl]-5-isoxazolyl}-ethanol

: 1268385-39-2
1,1-dimethylethyl {3-[4-(propyloxy)-2-(trifluoromethyl)phenyl]-5-isoxazolyl}acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: periodic acid / acetonitrile / 0 - 20 °C

1.2: 0 - 20 °C

2.1: sulfuric acid / isopropyl alcohol; diethyl ether; water / 20 °C / Cooling with dry ice

With sulfuric acid; periodic acid; In diethyl ether; water; isopropyl alcohol; acetonitrile;