(L)-menthyl 1-carboethoxy-3-<<2-methoxymethyloxy>ethyl>-3-nitro-4-piperidine acetate

Base Information

Chemical Name:(L)-menthyl 1-carboethoxy-3-<<2-methoxymethyloxy>ethyl>-3-nitro-4-piperidine acetate
CAS No.:155339-59-6
Molecular Formula:C₂₄H₄₂N₂O₈
Molecular Weight:486.606
Hs Code.:

Synonyms:(L)-menthyl 1-carboethoxy-3-<<2-methoxymethyloxy>ethyl>-3-nitro-4-piperidine acetate

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Chemical Property of (L)-menthyl 1-carboethoxy-3-<<2-methoxymethyloxy>ethyl>-3-nitro-4-piperidine acetate

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Technology Process of (L)-menthyl 1-carboethoxy-3-<<2-methoxymethyloxy>ethyl>-3-nitro-4-piperidine acetate

There total 8 articles about (L)-menthyl 1-carboethoxy-3-<<2-methoxymethyloxy>ethyl>-3-nitro-4-piperidine acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 541-41-3
chloroformic acid ethyl ester

: (L)-menthyl N-benzyl-<3-(2-methoxymethyloxy)ethyl>-3-nitro-4-piperidine acetate

: (L)-menthyl 1-carboethoxy-3-<<2-methoxymethyloxy>ethyl>-3-nitro-4-piperidine acetate

: 155339-59-6
(L)-menthyl 1-carboethoxy-3-<<2-methoxymethyloxy>ethyl>-3-nitro-4-piperidine acetate

Guidance literature:: In benzene; for 24h; Heating;
DOI:10.1016/S0040-4020(01)86974-X

Reference yield:

: 75468-48-3
(L)-carbomenthyloxymethyl triphenylphosphonium bromide

: 155339-59-6
(L)-menthyl 1-carboethoxy-3-<<2-methoxymethyloxy>ethyl>-3-nitro-4-piperidine acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 57.6 percent / potassium t-butoxide / benzene; dioxane / 2.5 h / 25 °C

2: 87.3 percent / trifluoroacetic acid / CH₂Cl₂ / 0 °C

3: 36 percent / K₂CO₃ / ethanol / 108 h / 25 °C

4: 85 percent / ammonium acetate / ethanol / 60 h / 25 °C

5: 72 percent / benzene / 24 h / Heating

With ammonium acetate; potassium tert-butylate; potassium carbonate; trifluoroacetic acid; In 1,4-dioxane; ethanol; dichloromethane; benzene;
DOI:10.1016/S0040-4020(01)86974-X

Reference yield:

: 155339-55-2
4-methoxymethyloxy-2-nitrobutan-1-ol

: 155339-59-6
(L)-menthyl 1-carboethoxy-3-<<2-methoxymethyloxy>ethyl>-3-nitro-4-piperidine acetate

Guidance literature:: Multi-step reaction with 4 steps

1: 79.3 percent / pyridine / CH₂Cl₂ / 0.17 h / 0 °C

2: 36 percent / K₂CO₃ / ethanol / 108 h / 25 °C

3: 85 percent / ammonium acetate / ethanol / 60 h / 25 °C

4: 72 percent / benzene / 24 h / Heating

With pyridine; ammonium acetate; potassium carbonate; In ethanol; dichloromethane; benzene;
DOI:10.1016/S0040-4020(01)86974-X