Phosphoric acid mono-{2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl} ester

Base Information

Chemical Name:Phosphoric acid mono-{2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl} ester
CAS No.:183867-91-6
Molecular Formula:C₂₀H₂₆NO₆P
Molecular Weight:407.403
Hs Code.:

Synonyms:Phosphoric acid mono-{2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl} ester

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Chemical Property of Phosphoric acid mono-{2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl} ester

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Technology Process of Phosphoric acid mono-{2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl} ester

There total 4 articles about Phosphoric acid mono-{2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl} ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 183867-84-7
Phosphoric acid dibenzyl ester 2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl ester

: 183867-91-6
Phosphoric acid mono-{2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl} ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; for 12h;
DOI:10.1021/jo961477p

Reference yield:

: 134098-64-9
2‐{3‐[(O‐tert‐butyldimethylsilyl)hydroxy]‐1,1‐dimethylpropyl}‐3,5‐dimethylphenol

: 183867-91-6
Phosphoric acid mono-{2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl} ester

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / potassium tert-butoxide / tetrahydrofuran / 0.75 h / 60 °C

2: 72 percent / KF, Jones reagent / acetone

3: 67 percent / 4-DMAP, EDC / CH₂Cl₂ / 24 h / 0 - 20 °C

4: 77 percent / H₂ / Pd/C / tetrahydrofuran / 12 h

With dmap; potassium fluoride; jones reagent; potassium tert-butylate; hydrogen; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/jo961477p

Reference yield:

: 153910-62-4
3-(2-((bis(benzyloxy)phosphoryl)oxy)-4,6-dimethylphenyl)-3-methylbutanoic acid

: 183867-91-6
Phosphoric acid mono-{2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl} ester

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / 4-DMAP, EDC / CH₂Cl₂ / 24 h / 0 - 20 °C

2: 77 percent / H₂ / Pd/C / tetrahydrofuran / 12 h

With dmap; hydrogen; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo961477p