Phosphoric acid dibenzyl ester 2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl ester

Base Information

Chemical Name:Phosphoric acid dibenzyl ester 2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl ester
CAS No.:183867-84-7
Molecular Formula:C₃₄H₃₈NO₆P
Molecular Weight:587.653
Hs Code.:

Synonyms:Phosphoric acid dibenzyl ester 2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl ester

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Chemical Property of Phosphoric acid dibenzyl ester 2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl ester

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Technology Process of Phosphoric acid dibenzyl ester 2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl ester

There total 4 articles about Phosphoric acid dibenzyl ester 2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 104-94-9
4-methoxy-aniline

: 153910-62-4
3-(2-((bis(benzyloxy)phosphoryl)oxy)-4,6-dimethylphenyl)-3-methylbutanoic acid

: 183867-84-7
Phosphoric acid dibenzyl ester 2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl ester

Guidance literature:: With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; at 0 - 20 ℃; for 24h;
DOI:10.1021/jo961477p

Reference yield:

: 990-91-0
dibenzyl [[bis(benzyloxy)phosphoryl]oxy]phosphonate

: 183867-84-7
Phosphoric acid dibenzyl ester 2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / potassium tert-butoxide / tetrahydrofuran / 0.75 h / 60 °C

2: 72 percent / KF, Jones reagent / acetone

3: 67 percent / 4-DMAP, EDC / CH₂Cl₂ / 24 h / 0 - 20 °C

With dmap; potassium fluoride; jones reagent; potassium tert-butylate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/jo961477p

Reference yield:

: 134098-64-9
2‐{3‐[(O‐tert‐butyldimethylsilyl)hydroxy]‐1,1‐dimethylpropyl}‐3,5‐dimethylphenol

: 183867-84-7
Phosphoric acid dibenzyl ester 2-[2-(4-methoxy-phenylcarbamoyl)-1,1-dimethyl-ethyl]-3,5-dimethyl-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / potassium tert-butoxide / tetrahydrofuran / 0.75 h / 60 °C

2: 72 percent / KF, Jones reagent / acetone

3: 67 percent / 4-DMAP, EDC / CH₂Cl₂ / 24 h / 0 - 20 °C

With dmap; potassium fluoride; jones reagent; potassium tert-butylate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/jo961477p