trichloro(trimethylamine)boron

Base Information

• Chemical Name: trichloro(trimethylamine)boron
• CAS No.: 1516-55-8
• Molecular Formula: C3H9 B Cl3 N
• Molecular Weight: 176.281
• Mol file: 1516-55-8.mol

Synonyms:Methanamine,N,N-dimethyl-, compd. with trichloroborane (1:1); Trimethylamine, compd. withBCl3 (6CI,7CI); Trimethylamine, compd. with boron chloride (BCl3) (1:1) (8CI);Borane, trichloro-, compd. with N,N-dimethylmethanamine (1:1); Boron chloride(BCl3), compd. with trimethylamine (1:1) (8CI); Boron trichloride compound withtrimethylamine (1:1); Trimethylamine compd. with boron trichloride (1:1);Trimethylamine compound with trichloroborane (1:1);Trimethylamine-trichloroborane (1:1) adduct

Chemical Property of trichloro(trimethylamine)boron

Chemical Property:

• Vapor Pressure: 1720mmHg at 25°C
• Melting Point: 237-240℃ (decomposition)
• Boiling Point: 2.8°Cat760mmHg
• Flash Point: °C
• PSA: 3.24000
• Density: g/cm³
• LogP: -9.99410

Purity/Quality:

99.9% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of trichloro(trimethylamine)boron

There total 11 articles about trichloro(trimethylamine)boron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

trimethylamine-borane (75-22-9) + boron trichloride (10294-34-5) → Me3NBCl3 (1516-55-8)

Guidance literature:

heating for 12h;;

Reference yield:

boron trichloride (10294-34-5) → Me3NBCl3 (1516-55-8)

Guidance literature:

With trimethylamine; In benzene; (CH3)3N is bubbled through a soln. of BCl3 in benzene; recrystn. (benzene-chloroform);

DOI:10.1016/0022-2860(93)07913-H

Reference yield:

trimethylamine-borane (75-22-9) + mercury dichloride → Me3NBCl3 (1516-55-8) + (CH3)3N*BHCl2 (25741-83-7)

Guidance literature:

In neat (no solvent); excess HgCl2, 150°C, 35h;; product mixture;;

DOI:10.1016/S0020-1693(00)93235-3

upstream raw materials:

thionyl chloride

trimethylamine-borane

boron trichloride

sulfuryl dichloride

Downstream raw materials:

trimethylamine-borane