N-tert-butyl-N-{N'-[[(9-fluorenylmethyl)oxy]carbonyl]-L-alanoyl}-O-benzoylhydroxylamine

Base Information

Chemical Name:N-tert-butyl-N-{N'-[[(9-fluorenylmethyl)oxy]carbonyl]-L-alanoyl}-O-benzoylhydroxylamine
CAS No.:280137-56-6
Molecular Formula:C₂₉H₃₀N₂O₅
Molecular Weight:486.568
Hs Code.:

Synonyms:N-tert-butyl-N-{N'-[[(9-fluorenylmethyl)oxy]carbonyl]-L-alanoyl}-O-benzoylhydroxylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-tert-butyl-N-{N'-[[(9-fluorenylmethyl)oxy]carbonyl]-L-alanoyl}-O-benzoylhydroxylamine

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Technology Process of N-tert-butyl-N-{N'-[[(9-fluorenylmethyl)oxy]carbonyl]-L-alanoyl}-O-benzoylhydroxylamine

There total 3 articles about N-tert-butyl-N-{N'-[[(9-fluorenylmethyl)oxy]carbonyl]-L-alanoyl}-O-benzoylhydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35661-39-3,136132-75-7
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine

: 280137-56-6
N-tert-butyl-N-{N'-[[(9-fluorenylmethyl)oxy]carbonyl]-L-alanoyl}-O-benzoylhydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: DMF / CH₂Cl₂ / 1.5 h / Heating

2: 1.56 g / pyridine / benzene / Heating

With pyridine; N,N-dimethyl-formamide; In dichloromethane; benzene; 1: Substitution / 2: Condensation;
DOI:10.1021/ol005722+

Reference yield:

: 94-36-0
dibenzoyl peroxide

: 280137-56-6
N-tert-butyl-N-{N'-[[(9-fluorenylmethyl)oxy]carbonyl]-L-alanoyl}-O-benzoylhydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / benzene / 45 °C

2: 1.56 g / pyridine / benzene / Heating

With pyridine; In benzene; 1: Disproportionation / 2: Condensation;
DOI:10.1021/ol005722+