2-[3-(3-bromophenyl)-2-(S-t-butylsulfanylmethyl)propionylamino]acetic acid benzyl ester

Base Information

• Chemical Name: 2-[3-(3-bromophenyl)-2-(S-t-butylsulfanylmethyl)propionylamino]acetic acid benzyl ester
• CAS No.: 1162122-12-4
• Molecular Formula: C₂₃H₂₈BrNO₃S
• Molecular Weight: 478.45

Synonyms:2-[3-(3-bromophenyl)-2-(S-t-butylsulfanylmethyl)propionylamino]acetic acid benzyl ester

Chemical Property of 2-[3-(3-bromophenyl)-2-(S-t-butylsulfanylmethyl)propionylamino]acetic acid benzyl ester

Chemical Property:

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Technology Process of 2-[3-(3-bromophenyl)-2-(S-t-butylsulfanylmethyl)propionylamino]acetic acid benzyl ester

There total 1 articles about 2-[3-(3-bromophenyl)-2-(S-t-butylsulfanylmethyl)propionylamino]acetic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

2-(S-t-butylsulfanylmethyl)-3-(3-bromophenyl)propionic acid (1162122-11-3) + benzyl 2-aminoacetate hydrochloride (2462-31-9) → 2-[3-(3-bromophenyl)-2-(S-t-butylsulfanylmethyl)propionylamino]acetic acid benzyl ester (1162122-12-4)

Guidance literature:

With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃;

DOI:10.1002/jlcr.1566

Reference yield:

2-[3-(3-bromophenyl)-2-(S-t-butylsulfanylmethyl)propionylamino]acetic acid benzyl ester (1162122-12-4) → S-t-butylthiorphan + C16H22(2)HNO3S (1162122-13-5)

Guidance literature:

With palladium on activated charcoal; deuterium; In ethyl acetate;

DOI:10.1002/jlcr.1566

Reference yield:

2-[3-(3-bromophenyl)-2-(S-t-butylsulfanylmethyl)propionylamino]acetic acid benzyl ester (1162122-12-4) → C16H22(3)HNO3S (1162122-14-6)

Guidance literature:

With tritium; 20% Pd(OH)2/C; triethylamine; In water; for 5h;

DOI:10.1002/jlcr.1566

upstream raw materials:

2-(S-t-butylsulfanylmethyl)-3-(3-bromophenyl)propionic acid

benzyl 2-aminoacetate hydrochloride

Downstream raw materials:

C₁₆H₂₂⁽²⁾HNO₃S

C₁₆H₂₂⁽³⁾HNO₃S

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