ethyl (+/-)-3-{[3-({4-[(3-aminopropyl)amino]butyl}amino)propyl]amino}-3-phenylpropanoate

Base Information

Chemical Name:ethyl (+/-)-3-{[3-({4-[(3-aminopropyl)amino]butyl}amino)propyl]amino}-3-phenylpropanoate
CAS No.:174320-09-3
Molecular Formula:C₂₁H₃₈N₄O₂
Molecular Weight:378.558
Hs Code.:

Synonyms:ethyl (+/-)-3-{[3-({4-[(3-aminopropyl)amino]butyl}amino)propyl]amino}-3-phenylpropanoate

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Chemical Property of ethyl (+/-)-3-{[3-({4-[(3-aminopropyl)amino]butyl}amino)propyl]amino}-3-phenylpropanoate

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Technology Process of ethyl (+/-)-3-{[3-({4-[(3-aminopropyl)amino]butyl}amino)propyl]amino}-3-phenylpropanoate

There total 4 articles about ethyl (+/-)-3-{[3-({4-[(3-aminopropyl)amino]butyl}amino)propyl]amino}-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: ethyl 16-amino-3-phenyl-4,8,13-triaza-2-hexadecenoate

: 174320-09-3
ethyl (+/-)-3-{[3-({4-[(3-aminopropyl)amino]butyl}amino)propyl]amino}-3-phenylpropanoate

Guidance literature:: With hydrogen; platinum(IV) oxide; In ethanol; chloroform; at 25 ℃; for 12h;
DOI:10.1246/bcsj.71.1221

Reference yield:

: 71-44-3
Spermine

: 2216-94-6
phenylpropynoic acid ethyl ester

: 174320-09-3
ethyl (+/-)-3-{[3-({4-[(3-aminopropyl)amino]butyl}amino)propyl]amino}-3-phenylpropanoate

Guidance literature:: With chloroform; hydrogen; platinum(IV) oxide; Multistep reaction;
DOI:10.1021/ja953541a

Reference yield:

: 71-44-3
Spermine

: 174320-09-3
ethyl (+/-)-3-{[3-({4-[(3-aminopropyl)amino]butyl}amino)propyl]amino}-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / ethanol / 2 h / Heating

2: 68 percent / H₂ / platinum(IV) oxide / CHCl₃; ethanol / 12 h / 25 °C

With hydrogen; platinum(IV) oxide; In ethanol; chloroform; 1: Michael addition / 2: Catalytic hydrogenation;
DOI:10.1246/bcsj.71.1221