2,2-bis(benzyloxymethyl)-3-bromo-1-tert-butyldimethylsilyloxymethyl-3-fluorocyclopropane

Base Information

Chemical Name:2,2-bis(benzyloxymethyl)-3-bromo-1-tert-butyldimethylsilyloxymethyl-3-fluorocyclopropane
CAS No.:1012785-60-2
Molecular Formula:C₂₆H₃₆BrFO₃Si
Molecular Weight:523.558
Hs Code.:

Synonyms:2,2-bis(benzyloxymethyl)-3-bromo-1-tert-butyldimethylsilyloxymethyl-3-fluorocyclopropane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2-bis(benzyloxymethyl)-3-bromo-1-tert-butyldimethylsilyloxymethyl-3-fluorocyclopropane

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Technology Process of 2,2-bis(benzyloxymethyl)-3-bromo-1-tert-butyldimethylsilyloxymethyl-3-fluorocyclopropane

There total 1 articles about 2,2-bis(benzyloxymethyl)-3-bromo-1-tert-butyldimethylsilyloxymethyl-3-fluorocyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1868-53-7
dibromofluoromethane

: 552879-97-7
tert-Butyldimethylsilyl-3-benzyloxymethyl-4-benzyloxy-2-butenol

: 1012785-60-2
2,2-bis(benzyloxymethyl)-3-bromo-1-tert-butyldimethylsilyloxymethyl-3-fluorocyclopropane

Guidance literature:: With sodium hydroxide; tetra-(n-butyl)ammonium iodide; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1080/15257770701257210

Reference yield: 83.0%

: 1012785-60-2
2,2-bis(benzyloxymethyl)-3-bromo-1-tert-butyldimethylsilyloxymethyl-3-fluorocyclopropane

: 1012785-61-3
(+/-)-tert-Butyldimethylsilyl-[2,2-bis(benzyloxymethyl)-3-fluorocyclopropyl]methanol

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; for 4h; Heating;
DOI:10.1080/15257770701257210

Reference yield:

: 1012785-60-2
2,2-bis(benzyloxymethyl)-3-bromo-1-tert-butyldimethylsilyloxymethyl-3-fluorocyclopropane

: 604785-90-2
2,2-bis(benzyloxymethyl)-3-fluoro-1-(hydroxymethyl)cyclopropane

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / AIBN; Bu₃SnH / 4 h / Heating

2: 94 percent / Bu₄NF / tetrahydrofuran / 8 h / 20 °C

With 2,2'-azobis(isobutyronitrile); tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; In tetrahydrofuran;
DOI:10.1080/15257770701257210