10-dimethyl-aminophenyl-5-fluoro-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide

Base Information

Chemical Name:10-dimethyl-aminophenyl-5-fluoro-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide
CAS No.:1357002-73-3
Molecular Formula:C₂₇H₂₉BFN₃
Molecular Weight:425.357
Hs Code.:

Synonyms:10-dimethyl-aminophenyl-5-fluoro-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide

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Chemical Property of 10-dimethyl-aminophenyl-5-fluoro-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide

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Technology Process of 10-dimethyl-aminophenyl-5-fluoro-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide

There total 4 articles about 10-dimethyl-aminophenyl-5-fluoro-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1334305-64-4
10-dimethyl-aminophenyl-5-hydroxyl-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide

: 1357002-73-3
10-dimethyl-aminophenyl-5-fluoro-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide

Guidance literature:: With potassium hydrogen difluoride; In tetrahydrofuran; for 24h; Inert atmosphere;
DOI:10.1039/c1cc13089g

Reference yield:

: 625-82-1
2,4-dimethyl-1H-pyrrole

: 1357002-73-3
10-dimethyl-aminophenyl-5-fluoro-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C / Inert atmosphere

1.2: 0.25 h / 20 °C / Inert atmosphere

1.3: 20 °C / Inert atmosphere

2.1: potassium hydrogen difluoride / tetrahydrofuran / 24 h / Inert atmosphere

With potassium hydrogen difluoride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c1cc13089g

Reference yield:

: 873-51-8
phenylborondichloride

: 1357002-73-3
10-dimethyl-aminophenyl-5-fluoro-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C / Inert atmosphere

1.2: 0.25 h / 20 °C / Inert atmosphere

1.3: 20 °C / Inert atmosphere

2.1: potassium hydrogen difluoride / tetrahydrofuran / 24 h / Inert atmosphere

With potassium hydrogen difluoride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c1cc13089g