10-dimethyl-aminophenyl-5-hydroxyl-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide

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Chemical Name:10-dimethyl-aminophenyl-5-hydroxyl-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide
CAS No.:1334305-64-4
Molecular Formula:C₂₇H₃₀BN₃O
Molecular Weight:423.366
Hs Code.:

Synonyms:10-dimethyl-aminophenyl-5-hydroxyl-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide

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Chemical Property of 10-dimethyl-aminophenyl-5-hydroxyl-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide

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Technology Process of 10-dimethyl-aminophenyl-5-hydroxyl-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide

There total 1 articles about 10-dimethyl-aminophenyl-5-hydroxyl-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 625-82-1
2,4-dimethyl-1H-pyrrole

: 873-51-8
phenylborondichloride

: 100-10-7
4-dimethylamino-benzaldehyde

: 1334305-64-4
10-dimethyl-aminophenyl-5-hydroxyl-5-phenyl-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:1’,2’-f][1,3,2]diazaborinin-4-ium-5-uide

Guidance literature:: 2,4-dimethyl-1H-pyrrole; 4-dimethylamino-benzaldehyde; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;

With chloranil; In dichloromethane; at 20 ℃; for 0.25h; Inert atmosphere;

phenylborondichloride; With triethylamine; In diethyl ether; dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1039/c1cc13089g