3,3'-dichlorobenzilic acid

Base Information

• Chemical Name: 3,3'-dichlorobenzilic acid
• CAS No.: 85259-23-0
• Molecular Formula: C₁₄H₁₀Cl₂O₃
• Molecular Weight: 297.138

Synonyms:3,3'-dichlorobenzilic acid

Chemical Property of 3,3'-dichlorobenzilic acid

Chemical Property:

Purity/Quality:

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Technology Process of 3,3'-dichlorobenzilic acid

There total 3 articles about 3,3'-dichlorobenzilic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-bis(3-chlorophenyl)ethane-1,2-dione (35190-07-9) → 3,3'-dichlorobenzilic acid (85259-23-0)

Guidance literature:

With potassium hydroxide; butan-1-ol;

DOI:10.1039/jr9470000952

Reference yield:

tetrachloromethane (56-23-5) + 1,2-bis(3-chlorophenyl)ethane-1,2-dione (35190-07-9) → 3,3'-dichlorobenzilic acid (85259-23-0)

Guidance literature:

at 60.5 ℃; Rate constant; Umlagerung;

Reference yield:

→ 3,3'-dichlorobenzilic acid (85259-23-0)

Guidance literature:

upstream raw materials:

1,2-bis(3-chlorophenyl)ethane-1,2-dione

tetrachloromethane

Downstream raw materials:

bis(3-chlorophenyl)methanone

methyl 3,3'-dichlorobenzilate

5,5-Bis-(3-chloro-phenyl)-thiazolidine-2,4-dione

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