(E)-2-(2,4-dinitrophenyl)-N,N-dimethylethenamine

Base Information

• Chemical Name: (E)-2-(2,4-dinitrophenyl)-N,N-dimethylethenamine
• CAS No.: 1214-75-1
• Molecular Formula: C10H11 N3 O4
• Molecular Weight: 237.21
• Hs Code.: 2921499090
• European Community (EC) Number: 634-230-3
• Nikkaji Number: J2.247.510J
• Mol file: 1214-75-1.mol

Synonyms:61293-29-6;(E)-2-(2,4-dinitrophenyl)-N,N-dimethylethenamine;[(E)-2-(2,4-dinitrophenyl)ethenyl]dimethylamine;Ethenamine,2-(2,4-dinitrophenyl)-N,N-dimethyl-;2-(2,4-dinitrophenyl)-N,N-dimethyl-1-ethylenamine;1214-75-1;SCHEMBL8957884;HMS559I16;CCG-48166;MFCD00024408;AKOS005100594;8B-089;2-(2,4-Dinitrophenyl)-N,N-dimethylethen-1-amine;SR-01000637730-1;(N,N-Dimethylamino)ethenyl-2,4-dinitrobenzene, >=97%

Chemical Property of (E)-2-(2,4-dinitrophenyl)-N,N-dimethylethenamine

Chemical Property:

• Vapor Pressure: 2.82E-05mmHg at 25°C
• Melting Point: 163-167 °C(lit.)
• Refractive Index: 1.633
• Boiling Point: 356.9°C at 760 mmHg
• Flash Point: 169.7°C
• PSA: 94.88000
• Density: 1.333g/cm³
• LogP: 3.08170
• XLogP3: 2.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 2
• Exact Mass: 237.07495584
• Heavy Atom Count: 17
• Complexity: 319

Purity/Quality:

99%+ ^*data from raw suppliers

N,N-Dimethyl-2,4-dinitrostyrylamine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C=CC1=C(C=C(C=C1)[N+](=O)[O-])[N+](=O)[O-]
• Isomeric SMILES: CN(C)/C=C/C1=C(C=C(C=C1)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of (E)-2-(2,4-dinitrophenyl)-N,N-dimethylethenamine

There total 3 articles about (E)-2-(2,4-dinitrophenyl)-N,N-dimethylethenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2,4-dinitrotoluene (121-14-2) + N,N-dimethyl-formamide dimethyl acetal (4637-24-5) → 2,4-Dinitro-ω-dimethylamino-styrol (1214-75-1)

Guidance literature:

In N,N-dimethyl-formamide; for 2h; Heating;

DOI:10.1007/s11178-005-0374-9

Reference yield:

2,4-dinitrotoluene (121-14-2) + N1,N1-dimethyl-N2-phenylformamidine (1783-25-1) → 2,4-Dinitro-ω-dimethylamino-styrol (1214-75-1)

Guidance literature:

at 130 - 140 ℃;

Reference yield:

2,4-dinitrotoluene (121-14-2) + N,N-dimethylformamide diethyl diacetal (1188-33-6) → 2,4-Dinitro-ω-dimethylamino-styrol (1214-75-1)

Guidance literature:

upstream raw materials:

2,4-dinitrotoluene

N₁,N₁-dimethyl-N₂-phenylformamidine

N,N-dimethylformamide diethyl diacetal

N,N-dimethyl-formamide dimethyl acetal