{(η5-C5Me5)Os(CO)(PMe2Ph)Br}

Base Information

Chemical Name:{(η5-C5Me5)Os(CO)(PMe2Ph)Br}
CAS No.:107087-80-9
Molecular Formula:C₁₉H₂₆BrOOsP
Molecular Weight:571.493
Hs Code.:

Synonyms:{(η5-C5Me5)Os(CO)(PMe2Ph)Br}

Suppliers and Price of {(η5-C5Me5)Os(CO)(PMe2Ph)Br}

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of {(η5-C5Me5)Os(CO)(PMe2Ph)Br}

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of {(η5-C5Me5)Os(CO)(PMe2Ph)Br}

There total 12 articles about {(η5-C5Me5)Os(CO)(PMe2Ph)Br} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 116670-02-1
{(η5-C5Me5)Os(CO)(PMe2Ph)CH2Ph}

: mercury dibromide

: 107087-80-9
{(η5-C5Me5)Os(CO)(PMe2Ph)Br}

: 4109-72-2
PhCH₂HgBr

Guidance literature:: In dichloromethane-d2; (N2); electrophilic cleavage reaction by addn. of HgBr2 to a soln. of Cp*Os(CO)(PMe2Ph)CH2Ph in CD2Cl2;; not isolated, detected by NMR;;

Reference yield: 80.0%

: 81554-89-4
{(η5-C5Me5)Os(CO)2Br}

: 1184-78-7
trimethylamine-N-oxide

: 672-66-2
Dimethyl(phenyl)phosphine

: 107087-80-9
{(η5-C5Me5)Os(CO)(PMe2Ph)Br}

Guidance literature:: In dichloromethane; (N2); reflux the mixt. for 24 h;; pumping the soln. to dryness and dissolution of the residue in a hexane or petroleum ether/CH2Cl2 solvent mixt.; chromy. (alumina column, CH2Cl2/hexane); solvent removal under vacuum; elem. anal.;;

Reference yield: 78.0%

: 116670-00-9
{(η5-C5Me5)Os(CO)(PMe2Ph)Et}

: 7726-95-6
bromine

: 74-96-4
ethyl bromide

: 107087-80-9
{(η5-C5Me5)Os(CO)(PMe2Ph)Br}

Guidance literature:: In dichloromethane-d2; (N2); electrophilic cleavage reaction by addn. of bromine to a soln. of Cp*Os(CO)(PMe2Ph)Et in CD2Cl2;; not isolated, detected by NMR;;