methyl (1-diphenylmethylamino-1-phenyl-methyl) (2-methoxycarbonyl-propyl) phosphinate

Base Information

Chemical Name:methyl (1-diphenylmethylamino-1-phenyl-methyl) (2-methoxycarbonyl-propyl) phosphinate
CAS No.:359454-75-4
Molecular Formula:C₂₆H₃₀NO₄P
Molecular Weight:451.502
Hs Code.:

Synonyms:methyl (1-diphenylmethylamino-1-phenyl-methyl) (2-methoxycarbonyl-propyl) phosphinate

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Chemical Property of methyl (1-diphenylmethylamino-1-phenyl-methyl) (2-methoxycarbonyl-propyl) phosphinate

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Technology Process of methyl (1-diphenylmethylamino-1-phenyl-methyl) (2-methoxycarbonyl-propyl) phosphinate

There total 4 articles about methyl (1-diphenylmethylamino-1-phenyl-methyl) (2-methoxycarbonyl-propyl) phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7
methacrylic acid methyl ester

: 359454-74-3
methyl 1-diphenylmethylamino-1-phenyl-methyl phosphinate

: 359454-75-4
methyl (1-diphenylmethylamino-1-phenyl-methyl) (2-methoxycarbonyl-propyl) phosphinate

Guidance literature:: With sodium methylate; In methanol; at 0 - 24 ℃;
DOI:10.1016/S0040-4039(01)00768-7

Reference yield:

: 62506-88-1
N-benzylidenediphenylmethanamine

: 359454-75-4
methyl (1-diphenylmethylamino-1-phenyl-methyl) (2-methoxycarbonyl-propyl) phosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 1 h / Heating

2: t-BuOK / tetrahydrofuran

With potassium tert-butylate; In tetrahydrofuran; methanol; 2: Michael addition;
DOI:10.1080/10426500212259

Reference yield:

: 100-52-7
benzaldehyde

: 359454-75-4
methyl (1-diphenylmethylamino-1-phenyl-methyl) (2-methoxycarbonyl-propyl) phosphinate

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / methanol / 1 h / Heating

2: 87 percent / NaOMe / methanol / 0 - 24 °C

With sodium methylate; In methanol; 2: Kakachnik-Fields reaction / 3: Michael addition;
DOI:10.1016/S0040-4039(01)00768-7