2-hydroxyimino-3-oxo-3-phenyldithiopropionic acid methyl ester

Base Information

Chemical Name:2-hydroxyimino-3-oxo-3-phenyldithiopropionic acid methyl ester
CAS No.:1609182-70-8
Molecular Formula:C₁₀H₉NO₂S₂
Molecular Weight:239.319
Hs Code.:

Synonyms:2-hydroxyimino-3-oxo-3-phenyldithiopropionic acid methyl ester

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Chemical Property of 2-hydroxyimino-3-oxo-3-phenyldithiopropionic acid methyl ester

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Technology Process of 2-hydroxyimino-3-oxo-3-phenyldithiopropionic acid methyl ester

There total 2 articles about 2-hydroxyimino-3-oxo-3-phenyldithiopropionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 20365-21-3
methyl 3-oxo-3-phenylpropanedithioate

: 1609182-70-8
2-hydroxyimino-3-oxo-3-phenyldithiopropionic acid methyl ester

Guidance literature:: With hydrogenchloride; sodium nitrite; In methanol; at 0 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1021/acs.joc.7b01601

Reference yield: 91.0%

: 13636-68-5
methyl 3-hydroxy-3-phenylprop-2-enedithioate

: 1609182-70-8
2-hydroxyimino-3-oxo-3-phenyldithiopropionic acid methyl ester

Guidance literature:: With hydrogenchloride; sodium nitrite; In methanol; for 0.583333h; Cooling with ice;
DOI:10.1016/j.tet.2014.03.097

Reference yield: 90.0%

: 623-73-4
diazoacetic acid ethyl ester

: 1609182-70-8
2-hydroxyimino-3-oxo-3-phenyldithiopropionic acid methyl ester

: ethyl 4-benzoyl-5-(methylthio)thiazole-2-carboxylate

Guidance literature:: With tetrakis(actonitrile)copper(I) hexafluorophosphate; In dichloromethane; at 50 ℃; for 0.5h; Reagent/catalyst; Solvent; Temperature; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.joc.7b01601