C₂₀H₂₀O₈

Base Information

Chemical Name:C₂₀H₂₀O₈
CAS No.:1430416-85-5
Molecular Formula:C₂₀H₂₀O₈
Molecular Weight:388.374
Hs Code.:

C<sub>20</sub>H<sub>20</sub>O<sub>8</sub>

Synonyms:C₂₀H₂₀O₈

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Chemical Property of C₂₀H₂₀O₈

Chemical Property:

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Technology Process of C₂₀H₂₀O₈

There total 8 articles about C₂₀H₂₀O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1430417-55-2
(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-dihydroxyphenyl)acrylate

: 1430416-85-5
C₂₀H₂₀O₈

Guidance literature:: With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.ejmech.2012.09.047

Reference yield:

: 143815-52-5
(Z)-3-(3,4-dimethoxyphenyl)-2-hydroxyacrylic acid

: 1430416-85-5
C₂₀H₂₀O₈

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide; sodium tetrahydroborate / methanol / 0 - 20 °C / pH 10

2: toluene-4-sulfonic acid / toluene / 10 h / 100 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 24 h / 20 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; morpholine / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With morpholine; dmap; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1016/j.ejmech.2012.09.047

Reference yield:

: 331-39-5,501-16-6
caffeic acid

: 1430416-85-5
C₂₀H₂₀O₈

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 24 h / 20 °C / Inert atmosphere

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 24 h / 20 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; morpholine / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With morpholine; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.ejmech.2012.09.047